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1.
Bioactive compounds and antioxidant activities of the Korean lotus leaf (Nelumbo nucifera) condiment: volatile and nonvolatile metabolite profiling during fermentation
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Recent studies have shown that lotus (Nelumbo nucifera) leaf has various pharmacological effects. However, there have been no scientific investigations into these leaves as a fermented crude liquid. This study compared the in vitro antioxidant capacity of lotus leaf‐fermented broth (LLFB) with that of 57° Brix sugar broth (SB) as a control over a period of 6 months based on 1,1‐diphenyl‐2‐picrylhydrazyl radical scavenging activity, ferric ion reducing power, superoxide dismutase‐like activity, tyrosinase inhibition and nitrite scavenging activity. The dominant species during fermentation process were Leuconostoc lactis and Saccharomyces cerevisiae for LLFB. A total of thirty‐six metabolites such as alkaloids, fatty acids, organic acids, phenolics, sugar and sugar derivatives, ethyl esters and monoterpenoids differed between SB and LLFB using gas chromatography–mass spectrometry. Meanwhile, nine volatile compounds in LLFB contributed pleasant, slightly sweetish and fruity odour of condiment and sensory evaluation score of 4.06 ± 1.52 in the proportion of 1:9 LLFB/water. 相似文献
2.
数字下变频器GC1012B原理及配置方法 总被引:1,自引:0,他引:1
数字下变频技术是软件无线电的一项核心技术,其性能的好坏直接影响数字接收机的精度。GC1012B是美国TI公司推出的新型数字下变频器。文中从GC1012B的结构特点和内部功能框图出发,分析其工作原理,并介绍GC1012B几个主要寄存器的配置方法,从而实现对频率、滤波模式、增益大小等参数的设置。最后给出了一个具体配置实例作为参考。 相似文献
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4.
Guo Haitao Qiao Weihong Ba Yan Li Zongshi Jin Kun Peng Qinji 《Petroleum Science and Technology》2006,24(1):51-60
The GC/MS and NMR analysis of the reaction products of naphthalene with 1-bromohexane were reported. The products obtained were suggested to have six isomers of linear hexylnaphthalene and the structure of each isomer was determined by GC/MS and NMR spectra. For the first time, the unique chemical shift data were obtained. The content of each isomer calculated by 1H NMR and 13C NMR spectra was consistent with that by GC/MS spectra, which confirmed the accuracy of NMR data. 相似文献
5.
采用SE 3 0为固定液进行色谱柱分离 ,用外标定量法测定泥土中的微量六氯环戊二烯 ,结果最小检知量为 0 .18× 10 - 6 ,相关系数为 0 .99992。 相似文献
6.
为区分不同档次的玫瑰油,利用GC/MS法对高、中档玫瑰油进行了化学成分的定性和定量分析,分别鉴定出63和72种化合物。并对这2种玫瑰油和1种待测样品进行了电子香味扫描,确定电子鼻在玫瑰油档次辨别中的作用。 相似文献
7.
Giuseppe G. G. Manzardo Sandra Kürsteiner-Laube und Daniel Perrin 《Zeitschrift für Lebensmitteluntersuchung und -Forschung A》1996,203(6):501-506
In diethyl ether extracts from celeriac (Apium graveolens L. var.rapaceum) all four stereoisomers of (3a–7a)-cis-3-butylhexahydrophthalide were found to be present. The analyses were carried out by means of GC, enantioselective GC and GC-MS. The assignment of the relative configuration of the diastereomers3 and4 was accomplished by NOE difference spectroscopy. 相似文献
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9.
R.A. Jacques J.G. Santos C. Dariva J. Vladimir Oliveira E.B. Caramo 《The Journal of Supercritical Fluids》2007,40(3):354-359
This work presents a study concerning the chemical characteristics and analytical separation process of the essential oil obtained from high-pressure carbon dioxide extraction of Ilex paraguariensis. The experiments were performed in a laboratory-scale unit in the temperature range of 20–40 °C, from 100 to 250 bar. A blend of the I. paraguariensis extracts was percolated through a preparative chromatographic column, containing silica gel, and successively eluted with 150 mL of each of the following solvents: hexane, toluene, dichloromethane, ethyl acetate, acetone and methanol. The raw extract and its fractions were analyzed by gas chromatography coupled to mass spectrometry detection (GC/MS). The fractionation procedure showed to be a good clean up technique due to the isolation of different classes of compounds in each fraction. Chromatographic analyses allowed the identification of caffeine, fatty acids and esters, phytol, squalene, Vitamin E, stigmasterol derivatives and saturated hydrocarbons. 相似文献
10.
灭蚊窗涂剂的毛细管柱气相色谱分析 总被引:2,自引:2,他引:0
介绍了用AT-101毛细管柱,以邻苯二甲酸二正戊酯为内标,对灭蚊窗涂剂中3种有效成分残杀威、氯菊酯、氯氰菊酯同柱同条件下定量分析的方法。该方法的分析时间短,准确度、精密度高,重现性好。 相似文献