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1.
《International Journal of Hydrogen Energy》2022,47(63):27023-27031
Hexagonal boron nitride (h-BN) as a layered inorganic nonmetallic material has been widely used. Hydrogen peroxide (H2O2) modification can trigger exfoliation and afford abundant B–OH active sites at edge of h-BN, which can enhance methane activation ability. Introducing tungsten oxide (WO3) to h-BN produces a similar effect, because doping WO3 into h-BN resulted in electron transfer to N, inducing fracture of B–N bond, resulting in N vacancy (triboron center), exposing more B sites and promoting the generation of B–OH. Significantly, the introduction of WO3 on the modified h-BN dramatically increased the concentration of B–OH compared with the unmodified h-BN, because H2O2 modification weakened B–N bond. By means of XRD, TEM, XPS,EPR, FT-IR, it is proved that the high concentration of B–OH active sites contributed to activating C–H bond, thus methane conversion and CO and H2 selectivity were significantly improved. 相似文献
2.
Partial Discharge (PD) measurement is a globally accepted method for insulation diagnosis of electrical assets. The consequences of insulation breakdown are well known. The trend is to move from conventional offline testing to online monitoring for insulation life prediction, which results in the inclusion of high frequency noise in the captured signals. Therefore de-noising is of paramount importance in online monitoring to obtain useful information from the signal.In this research, a 20 kV switchgear panel has been subjected to PD faults in the laboratory and measurements have been carried out by using different non-intrusive sensors including a novel sensor, the D-dot sensor and recorded by a high frequency oscilloscope. The measured results show the effective applicability of sensors for switchgear. The Discrete Wavelet Transform (DWT) has been used to de-noise PD signals in this paper. Time domain and frequency domain comparison of original and de-noised PD signals reveals the significance of this technique for online monitoring of Medium Voltage (MV) switchgear. Finally, an adaptive online de-noising concept, based on automatic de-noising is also proposed in this paper. 相似文献
3.
Fresh and frozen-thawed (F-T) pork meats were classified by Vis–NIR hyperspectral imaging. Eight optimal wavelengths (624, 673, 460, 588, 583, 448, 552 and 609 nm) were selected by successive projections algorithm (SPA). The first three principal components (PCs) obtained by principal component analysis (PCA) accounted for over 99.98% of variance. Gray-level-gradient co-occurrence matrix (GLGCM) was applied to extract 45 textural features from the PC images. The correct classification rate (CCR) was employed to evaluate the performance of the partial least squares-discriminate analysis (PLS-DA) models, by using (A) the reflected spectra at full wavelengths and (B) those at the optimal wavelengths, (C) the extracted textures based on the PC images, and (D) the fused variables combining spectra at the optimal wavelengths and textures. The results showed that the best CCR of 97.73% was achieved by applying (D), confirming the high potential of textures for fresh and F-T meat discrimination. 相似文献
4.
This article presents a new approach for solving the Optimal Control Problem (OCP) of linear time-delay systems with a quadratic cost functional. The proposed method can also be used for designing optimal control time-delay systems with disturbance. In this study, the Variational Iteration Method (VIM) is employed to convert the original Time-Delay Optimal Control Problem (TDOCP) into a sequence of nonhomogeneous linear two-point boundary value problems (TPBVPs). The optimal control law obtained consists of an accurate linear feedback term and a nonlinear compensation term which is the limit of an adjoint vector sequence. The feedback term is determined by solving Riccati matrix differential equation. By using the finite-step iteration of a nonlinear compensation sequence, we can obtain a suboptimal control law. Finally, Illustrative examples are included to demonstrate the validity and applicability of the technique. 相似文献
5.
We extend the definition of the classical Jacobi polynomials withindexes α, β>−1 to allow α and/or β to be negative integers. We show that the generalized Jacobi polynomials, with indexes corresponding to the number of boundary conditions in a given partial differential equation, are the natural basis functions for the spectral approximation of this partial differential equation. Moreover, the use of generalized Jacobi polynomials leads to much simplified analysis, more precise error estimates and well conditioned algorithms.Mathematics subject classification 1991. 65N35, 65N22, 65F05, 35J05 相似文献
6.
This article addresses the computation of invariant control laws [A. Fradkov, I. Miroshnik, V. Nikiforov, Nonlinear and Adaptive Control of Complex Systems, Kluwer, 1999] for fed-batch fermenters represented by two standard models. It will be shown how to derive partial state feedbacks that, assuming ideal conditions and perfect model, keep the specific growth rate μ constant provided the initial conditions are adequate. The invariant control law is the closed loop version of the exponential feeding already suggested in several references as shown later. The paper presents an analysis of invariance and a study of global stability within the framework of partial stability. That is, stability with respect to some of the state variables. This enables us to treat the case with Haldane-like or non-monotonous kinetics. 相似文献
7.
C. Athanassiou G. Pekridis N. Kaklidis K. Kalimeri S. Vartzoka G. Marnellos 《International Journal of Hydrogen Energy》2007
In the present work, the prospects and trends of solid electrolyte membrane reactors (SEMRs) towards hydrogen production, are discussed. Initially, an overview of the principles, the properties and the techniques related to the usage of the SEMRs, are presented. In the following, a literature survey covering earlier and recent developments of the various methods (e.g. reforming or partial oxidation or dehydrogenation of hydrocarbons, steam electrolysis) employed in the SEMRs for the production of hydrogen, is performed. Finally, the current status of this research field is analyzed and future research topics are proposed. 相似文献
8.
利用沉降离心法将老虎山黄土-古土壤的酸不溶相分离成<2μm、2~45μm和>45μm三个粒级组分,并分别测定了这些组分和全岩的磁化率。结果表明,无论是全岩,还是三个不同粒级组分,它们的磁化率都可以单独作为长江中下游地区古气候演变的参考指标。其中,<2μm粒级的质量磁化率明显大于全岩和2~45μm、>45μm两粒级,而且其分辨率也明显高于2~45μm和>45μm这两个粒级组分。本实验结果还显示,虽然<2μum的质量磁化率最大,但对全岩质量磁化率的贡献率与2~45μm粒级相当,>45μm粒级的贡献率较低。 相似文献
9.
The partial oxidation of methanol to formaldehyde was studied over YBa2Cu3O7-x catalyst in a flow reactor. The structural change of YBa2Cu3O7-x before and after the reaction was measured by means of XRD and iodometric titration method. The catalytic characteristics
of YBa2Cu3O7-x for the partial oxidation of methanol to formaldehyde was due to copper ions. It was found that Cu+2 was responsible for the higher selectivity for formaldehyde. 相似文献
10.