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《Calphad》2021
The present work illustrates the effect of quasi-hydrostatic pressure on the positions and widths of the homogeneity ranges of the intermetallic phases TiFe and TiFe2 at high temperatures. The experiments were performed with Ti–Fe diffusion couples that were heat treated in a multi-anvil press at 2.5 GPa. The solubility limits of the phases were derived from the concentration profiles that were measured using electron probe microanalysis. It was found that the homogeneity ranges of TiFe and TiFe2 extend to higher titanium concentrations, if the pressure is applied. The positions of the phase boundaries of the intermetallics on the iron-rich side are not affected by the pressure. The accuracy of the experimental data including the homogeneity ranges and temperatures was verified by comparing the homogeneity ranges of β-Ti(Fe), α/δ-Fe(Ti) and γ-Fe measured in this study with the homogeneity ranges taken from literature. The pressure was calibrated using the pressure-induced phase transitions of bismuth. 相似文献
3.
Jialong Tian M. Babar Shahzad Wei Wang Lichang Yin Zhouhua Jiang Ke Yang 《材料科学技术学报》2018,34(9):1671-1675
The effect of Co addition on the formation of Ni-Ti clusters in maraging stainless steel was studied by three dimensional atom probe (3DAP) and first-principles calculation. The cluster analysis based on the maximum separation approach showed an increase in size but a decrease in density of Ni-Ti clusters with increasing the Co content. The first-principles calculation indicated weaker Co-Ni (Co-Ti) interactions than Co-Ti (Fe-Ti) interactions, which should be the essential reason for the change of distribution characteristics of Ni-Ti clusters in bcc Fe caused by Co addition. 相似文献
4.
P. G. Muzykov Y. I. Khlebnikov S. V. Regula Y. Gao T. S. Sudarshan 《Journal of Electronic Materials》2003,32(6):505-510
To establish fast, nondestructive, and inexpensive methods for resistivity measurements of SiC wafers, different resistivity-measurement
techniques were tested for characterization of semi-insulating SiC wafers, namely, the four-point probe method with removable
graphite contacts, the van der Pauw method with annealed metal and diffused contacts, the current-voltage (I-V) technique,
and the contactless resistivity-measurement method. Comparison of different techniques is presented. The resistivity values
of the semi-insulating SiC wafer measured using different techniques agree fairly well. As a result, application of removable
graphite contacts is proposed for fast and nondestructive resistivity measurement of SiC wafers using the four-point probe
method. High-temperature van der Pauw and room-temperature Hall characterization for the tested semi-insulating SiC wafer
was also obtained and reported in this work. 相似文献
5.
通过广西水电南宁地质勘探基础工程处推行职工持股的思路,结合广西水利施工企业目前的具体情况, 就如何推行职工持股进行探讨,并提出建议及看法。 相似文献
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The motional transition and heterogeneity of semi‐interpenetrating networks (SIPNs) based on polyurethane (PU) with carboxylic groups and methacrylic copolymer (PM) with tertiary amine groups were studied by the electron spin resonance (ESR) spin probe method. The concentration of functional groups in both prepolymers varied from 0 to 0.45 mmol g?1. Spin‐probed SIPNs show that the temperature‐dependent spectra are sensitive to polymer interactions imposed by functional groups. These interactions determine the free volume distribution in the matrix and temperature at which motional transition takes place. The fraction of free volume increases with functional group concentration and reaches its maximum at 0.25 mmol g?1. Further increases in the functional group concentration reduce the free volume. The results of the networks with strong interactions are discussed in terms of the interference of the plasticizing effect of the PU component and the formation of possible cluster cross‐links, which restricts segmental motions. Copyright © 2003 Society of Chemical Industry 相似文献
8.
介绍了用单根光纤传输测量信号和功率信号的光功率推动液体压力测量仪及其工作原理。该仪器以电容式压力传感器的δ元件作为压力检测元件,采用低功耗前置器电路和简单直杆结构,实现了便携式测量。测量范围为O~100kPa,精度为O.01kPa。 相似文献
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磷钨酸乙醇染色法在嗜铬颗粒电镜X射线显微分析中的应用 总被引:1,自引:0,他引:1
通过比较常规透射电镜制样法、快速冷冻固定-冷冻超薄切片法及磷钨酸乙醇(EPTA)染色法在嗜铬颗粒透射电镜X射线显微分析中的应用,发现磷钨酸乙醇染色法能使嗜铬颗粒电子着色,从而较好地显示嗜铬颗粒的超微结构。同时磷钨酸乙醇染色法也以在一定程度上原位保留生物样品中元素,可以应用于检测样品元素含量的变化或比较样品元素含量的组间差别,提示磷钨酸乙醇染色法是一种可应用于透射电镜X射线显微分析的经济简便的生物样品制备方法。 相似文献