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增溶胶束分光光度法测定蔬菜中锗的含量
引用本文:杜萌,王晓晖. 增溶胶束分光光度法测定蔬菜中锗的含量[J]. 辽宁化工, 2009, 38(3): 215-217
作者姓名:杜萌  王晓晖
作者单位:1. 唐山市纤维检验所,河北,唐山,063009
2. 邯钢集团有限公司,河北,邯郸,056015
摘    要:以苯芴酮为显色剂,吐温-80为表面活性剂,在HCl介质中与锗反应生成橙红色络合物,采用增溶胶束分光光度法测定蔬菜中锗的含量。以512nm为工作波长,并确定了实验所需最佳条件,采用HNO3-H2O2法消解蔬菜,测得蔬菜中锗的含量为1.54μg/g。

关 键 词:分光光度法    蔬菜  吐温-80  苯芴酮

Determination of Germanium Content in Vegetable by Spectrophotometry
DU Meng,WANG Xiao-hui. Determination of Germanium Content in Vegetable by Spectrophotometry[J]. Liaoning Chemical Industry, 2009, 38(3): 215-217
Authors:DU Meng  WANG Xiao-hui
Affiliation:1.Tangshan fiber Inspection;tangshan 063009;China;2.Handan Iron and Steel Group Co.Ltd;handan 056015;China
Abstract:Phenylfluorone can react with germanium to form an orange -red complex in the medium of hydrochloric acid. Using Phenylfluorone as colour developing reagent and Tween - 80 as surfactant, germanium content in vegetable was determined by pectrophotometry. The wave - length was 512 nm and optimium experiment conditions were confirmed. Vegetable was digested by HNO3 -H2O2 and the content of germanium was 1.54 μg/g.
Keywords:Speetrophotometry  Germanium ( IV )  Vegetable  Tween - 80  Phenylfluorone
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