| 2-乙氧基乙醇氨化合成2-乙氧基乙胺工艺研究 |
| |
| 引用本文： | 兰昭洪.2-乙氧基乙醇氨化合成2-乙氧基乙胺工艺研究[J].精细化工中间体,2008,38(6). |
| |
| 作者姓名： | 兰昭洪 |
| |
| 作者单位： | 新化高级胺省级高新技术研究开发中心,浙江,建德,311607 |
| |
| 摘 要： | 采用浸渍法制得Cu-Co-Ru-Mg-Cr/Al2O3催化剂,用于2-乙氧基乙醇氨化制备2-乙氧基乙胺反应;研究了反应压力、温度、空速、氨气与2-乙氧基乙醇摩尔比等因素对氨化反应的影响;在适宜的操作条件下,2-乙氧基乙醇单程转化率达到93%,2-乙氧基乙胺选择性达到95%。
|
| 关 键 词： | 2-乙氧基乙醇 2-乙氧基乙胺 氨化反应 |
Synthesis Process of 2-Ethoxyethylamine by Amination of 2-Ethoxyethanol |
| |
| LAN Zhao-hong.Synthesis Process of 2-Ethoxyethylamine by Amination of 2-Ethoxyethanol[J].Fine Chemical Intermediates,2008,38(6). |
| |
| Authors: | LAN Zhao-hong |
| |
| Affiliation: | LAN Zhao-hong (Provincial High-tech Research & Development Centre of Higher Carbon Amines (Xinhua),Ji,e 311607,China) |
| |
| Abstract: | A Cu -Co -Ru -Mg -Cr/Al2O3 catalyst was prepared by impregnation which was used to synthesize 2 - ethoxyethylamine by amination of 2-ethoxyethanol. Effects of the pressure, temperature, liquid space velocity, and mole ratio of ammoma and 2-ethoxyethanol on aminationf 2-ethoxyethanol was investigated. Under optimun reaction conditions, the conversion of 2-ethoxyethanol reached 93%, and the selectivity of 2- ethoxyethylamine reached 95%. |
| |
| Keywords: | 2-ethoxyethylamine 2-ethoxyethano amination |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
