| 均匀沉淀法制备纳米氧化锌的研究 |
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| 引用本文： | 汤皎宁,龚晓钟,李均钦. 均匀沉淀法制备纳米氧化锌的研究[J]. 无机材料学报, 2006, 21(1): 65-69 |
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| 作者姓名： | 汤皎宁 龚晓钟 李均钦 |
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| 作者单位： | 深圳大学理学院材料科学与工程系, 深圳市特种功能材料?重点实验室, 深圳 518060 |
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| 基金项目： | 广东省博士启动基金;广东省深圳市科技计划 |
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| 摘 要： | 以硝酸锌、尿素为原料, 采用均匀沉淀法制备纳米氧化锌粉末. 以TEM和BET等方法对产物进行了表征, 发现可获得50nm左右的纳米氧化锌, 粒子 的比表面积为25.6m2/g; XRD分析表明, 产物为六方晶系; 通过XRD、IR和TG-DSC分析, 确定了纳米氧化锌的形成机理.
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| 关 键 词： | 纳米氧化锌 均匀沉淀法 机理 |
| 文章编号： | 1000-324X（2006）01-0065-05 |
| 收稿时间： | 2005-01-04 |
| 修稿时间： | 2005-01-042005-04-22 |
Synthesis of Nanometer ZnO Particles by Directly Precipitation Method |
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| TANG Jiao-Ning,GONG Xiao-Zhong,LI Jun-Qin. Synthesis of Nanometer ZnO Particles by Directly Precipitation Method[J]. Journal of Inorganic Materials, 2006, 21(1): 65-69 |
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| Authors: | TANG Jiao-Ning GONG Xiao-Zhong LI Jun-Qin |
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| Affiliation: | Shenzhen Key Laboratory of Special Functional Materials, Material Department, College of Science, Shenzhen University, Shenzhen 518060, China |
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| Abstract: | Nanometer ZnO particles were synthesized by the homogeneous precipitation method from urea and zinc nitrate. TEM analysis shows that nanometer ZnO particles obtained are in the nanosize range of 50nm; BET analysis shows that the specific surface area of the ZnO particles is 25.6m^2/g; XRD analysis shows the crystalline of the nanometer ZnO particles is in the hexagonal structure; the formation mechanism of nanometer ZnO particles was concluded by the analysis of XRD, IR and TG-DSC. |
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| Keywords: | nano-zinc oxide homogeneous precipitation mechanism |
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