| 2，6─二氯苯酚的合成研究 |
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| 引用本文： | 张珩,杨建设,万江陵,陈芬儿. 2，6─二氯苯酚的合成研究[J]. 武汉化工学院学报, 1995, 0(1) |
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| 作者姓名： | 张珩 杨建设 万江陵 陈芬儿 |
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| 摘 要： | ４－羟基苯甲酸经气化、脱羧得２，６－二氯苯酚（１）。总收率６７．５％。通过均匀设计找到了氯化反应最佳实验条件。脱羧反应以三乙醇胺代替剧毒的Ｎ，Ｎ－二甲基苯胺，并对其后处理进行了改进。
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| 关 键 词： | 2，6－二氯苯酚，合成，氯化，脱羧 |
Studies on Synthesis of 2, 6-Dichlorophenol |
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| Zhang Heng, Yang Jianshe, Wan Jiangling, Chen Fen'er. Studies on Synthesis of 2, 6-Dichlorophenol[J]. Journal of Wuhan Institute of Chemical Technology, 1995, 0(1) |
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| Authors: | Zhang Heng Yang Jianshe Wan Jiangling Chen Fen'er |
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| Affiliation: | Zhang Heng; Yang Jianshe; Wan Jiangling; Chen Fen'er |
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| Abstract: | Dichlorophenol was synthesized from p-hydroxybenzoic acid in an overall yield of about 67. 5% via Chlorination and decarboxylation. The best experimental conditions of Chlorination have been found through uniform design. Triethanolamine was used instead of N,N-dimethylaniline in decarboxylation. |
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| Keywords: | Dichlorophenol Synthesis Chlorination Decarboxylation |
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