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烧结助剂添加方式对AlN陶瓷力学性能的影响
引用本文:许富民,李佳艳,张志军,石小磊,李晓娜,谭毅.烧结助剂添加方式对AlN陶瓷力学性能的影响[J].机械工程材料,2011(7).
作者姓名:许富民  李佳艳  张志军  石小磊  李晓娜  谭毅
作者单位:大连理工大学材料科学与工程学院辽宁省太阳能光伏系统重点实验室;
基金项目:国家自然科学基金资助项目(50871025); 辽宁省自然科学基金资助项目(20051075)
摘    要:通过直接添加与原位生成两种方式引入Y_2O_3作为烧结助剂,热压烧结制备了AlN陶瓷;研究了添加方式及添加量对AlN陶瓷显微结构和力学性能的影响。结果表明:原位生成烧结助剂的方式更有利于AlN陶瓷的致密化,特别是当原位生成的Y_2O_3质量分数为2%时,AlN陶瓷的相对密度达到99.0%,硬度为15.39GPa,抗弯强度为383.0MPa,均高于直接添加Y_2O_3的;同时可获得晶形完整、第二相含量少且大部分位于三叉晶界、晶粒间面-面接触的显微结构;随着原位生成烧结助剂添加量的增多,陶瓷的相对密度下降,在AlN晶界处出现大量第二相而导致陶瓷的硬度、抗弯强度等力学性能也下降。

关 键 词:AlN陶瓷  原位生成  烧结助剂  力学性能  

Effect of Adding Method of Sintering Additive on Mechanical Properties of AIN Ceramics
XU Fu-min,LI Jia-yan,ZHANG Zhi-jun,SHI Xiao-lei,LI Xiao-na,TAN Yi.Effect of Adding Method of Sintering Additive on Mechanical Properties of AIN Ceramics[J].Materials For Mechanical Engineering,2011(7).
Authors:XU Fu-min  LI Jia-yan  ZHANG Zhi-jun  SHI Xiao-lei  LI Xiao-na  TAN Yi
Affiliation:XU Fu-min,LI Jia-yan,ZHANG Zhi-jun,SHI Xiao-lei,LI Xiao-na,TAN Yi (Key Laboratory for Solar Energy Photovoltaic System of Liaoning Province,School of Materials Science and Engineering,Dalian University of Technology,Dalian 116024,China)
Abstract:AlN ceramics were fabricated by hot-pressing with Y_2O_3 as sintering additive added by direct addition and in-situ formation.The effects of adding method and amount of sintering additive on microstructure and mechanical properties of AlN ceramics were investigated.The results show that the sintering additive added by insitu formation was more beneficial to densification of AlN ceramics,and particularly,when Y_2O_3 was added by insitu formation and reached 2wt%.the relative density,hardness and flexural str...
Keywords:AlN ceramic  in-situ formation  sintering additive  mechanical property  
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