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Adhesion Science and Surface Analysis. Typical Examples
Authors:M. Romand   F. Gaillard  M. Charbonnier  N. S. Prakash  L. Deshayes  I. Linossier
Abstract:A number of surface modification methods using mechanical, chemical, electrochemical or physical processes have commonly been employed to treat adherend surfaces and improve adhesion in various bi- or multi-layered systems which play a key role in many advanced technologies. Results reported in this review paper deal more particularly with components of polymer-metal systems and provide typical examples of surface analysis obtained by x-ray photoelectron spectrometry (XPS), ion scattering spectrometry (ISS), low-energy electron induced x-ray spectrometry (LEEIXS), optically stimulated electron emission (OSEE) and Fourier transform infra-red spectrometry (FTIR). These examples concern, on the one hand, metallic adherends (aluminum, stainless steel, zinc-coated steel, gold) the surfaces of which were modified by cleaning, etching, oxidation, conversion or chemical grafting and, on the other hand, bonded joints (polyester-steel and epoxy-aluminum systems) which were delaminated using a peel test and a three-point flexure test, respectively.
Keywords:Surface analysis  XPS  ISS  FTIR  low energy electron induced spectrometry (LEEIXS)  optically stimulated electron emission (OSEE)  surface treatment  surface cleaning  surface etching  surface oxidation or conversion  surface grafting  adhesion science  metallic substrates  mechanical measurement  three-point flexure test  peel test  bonded joints
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