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辐照处理对柄曲霉素的降解效果研究
引用本文:赵亚荣,王琼珊,王旭,刘香香,王富华.辐照处理对柄曲霉素的降解效果研究[J].食品研究与开发,2020,41(14):34-37.
作者姓名:赵亚荣  王琼珊  王旭  刘香香  王富华
作者单位:广东省农业科学院农产品公共监测中心,广东广州510640;农业部农产品质量安全检测与评价重点实验室,广东广州 510640;广东食品药品职业学院,广东广州510520
摘    要:采用不同剂量(0、3、6、9、12、15 kGy)60Co-γ射线对柄曲霉素(sterigmatocystin,STC)溶液进行辐照处理,研究辐照剂量、不同溶剂以及不同初始浓度对柄曲霉素辐照降解效果的影响。结果表明:60Co-γ射线可有效降解溶液中的柄曲霉素,且降解率随着辐照剂量的增大而增加。当辐照剂量为3 kGy时,STC的降解速率依次为水>氯仿>乙腈>甲醇。当辐射剂量大于6 kGy时,水、乙腈和氯仿中STC的降解率相近,且甲醇中STC降解率也相对增加。在同一辐照剂量下,柄曲霉素的初始浓度越低,其降解率越高。

关 键 词:辐照  柄曲霉素  60Co-γ射线  降解  高效液相色谱-串联质谱
收稿时间:2019/7/18 0:00:00

Study on Degradation Effect of Irradiation on Sterigmatocystin
ZHAO Ya-rong,WANG Qiong-shan,WANG Xu,LIU Xiang-xiang,WANG Fu-hua.Study on Degradation Effect of Irradiation on Sterigmatocystin[J].Food Research and Developent,2020,41(14):34-37.
Authors:ZHAO Ya-rong  WANG Qiong-shan  WANG Xu  LIU Xiang-xiang  WANG Fu-hua
Affiliation:(Public Monitoring Center for Agro-product of Guangdong Academy of Agricultural Sciences,Guangzhou 510640,Guangdong,China;Key Laboratory of Testing and Evaluation for Agro-product Safety and Quality,Guangzhou 510640,Guangdong,China;Guangdong Food and Drug Vocational College,Guangzhou 510520,Guangdong,China)
Abstract:In this study,the solutions of sterigmatocystin(STC)were irradiated by different doses(0,3,6,9,12,15 kGy)60Co-γray radiation.The effects of irradiation dose,different solvents,initial concentrations on STC were investigated.The results showed that STC could be effectively degraded by 60Co-γray and the degradation rate increased with the increase of irradiation dose.The STC degradation rate was in the order of water>chloroform>acetonitrile>methanol when the irradiation dose was 3 kGy.Degradation rate in methanol was increased relatively and similar in water,acetonitrile and chloroform at the irradiation dose of greater than 6 kGy.At the same irradiation dose,the degradation rate was higher along with lower initial concentrations of STC.
Keywords:irradiation  sterigmatocystin  60Co-γray  degradation  high performance liquid chromatography-tandem mass spectrometry
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