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Note on the interpretation of powder shear test data
Authors:Jon Hilden  Keith Bowman  Steve Wang  Bryan Ennis
Affiliation:a Eli Lilly & Co., Indianapolis, IN, United States
b Materials Sci. and Eng. Department, Purdue University, West Lafayette, IN, United States
c Indust. Phys. Pharm. Department, Purdue University, West Lafayette, IN, United States
d Bristol-Myers Squibb, New Brunswick, NJ, United States
e E&G Associates, Nashville, TN, United States
Abstract:Powder shear testing has been used to assess flowability of powders for at least 48 years A.W. Jenike, Storage and Flow of Solids, Bull., Eng. Exp. Station, Univ. Utah, vol. 123, 1964]. A fundamental part of the data interpretation involves construction of Mohr’s circles such that they are tangent to the experimental locus; a set of powder shear strengths, τm, measured at variable applied compressive normal stresses, σN. Despite the customary application of this tangency criterion, we have found justifications for it to be scant.In this work, we revisit the Mohr’s circle construction and find that proper construction would require measurement of reactionary lateral powder stresses, σr. We further provide reasoning to support placement of the experimental locus passing through the apex (top) of Mohr’s circles for isotropic or orthotropic powders and not tangentially to them. This placement is not unexpectedly in agreement with the results of a recent numerical simulation C. Thornton, L. Zhang, Numerical simulations of the direct shear test, Chem. Eng. Technol. 26 (2) (2003) 153-156], and reveals errors in subsequently calculated constants on the order of 20%.
Keywords:Shear testing  Flow rules  Mohr's circles  Internal friction  Yield  Coulomb
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