| 相转移催化合成N,N—二乙基邻乙基苯胺的研究 |
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| 引用本文： | 孟艳秋,赵鸣玉.相转移催化合成N,N—二乙基邻乙基苯胺的研究[J].辽宁化工,1999,28(2):95-96. |
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| 作者姓名： | 孟艳秋 赵鸣玉 |
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| 作者单位： | 沈阳化工学院 |
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| 摘 要： | 在常压下以三乙基苄基氯化铵作相转移催化剂合成制得Ｎ，Ｎ－二乙基邻乙基苯胺，研究了各反应因素对目的产物产率的影响，其优化工艺条件为：在５０ｍｌ５０％的氢氧化钠溶液中，邻乙基苯胺和溴乙烷的摩尔比为１：２．６，三乙基苄基氯化铵用量为０．５０ｇ，反应回流时间１８．０ｈＮ，－烷基化反应的收率为５７．５％。
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| 关 键 词： | 二乙基 邻乙基苯胺 烷基化 相转移 催化 |
Study on the Synthesis of N,N-diethyl-o-ethylaniline in the Presence of Phase Transfer Catalysis |
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| Meng YanqiuZhao MingyuZhang Dayang.Study on the Synthesis of N,N-diethyl-o-ethylaniline in the Presence of Phase Transfer Catalysis[J].Liaoning Chemical Industry,1999,28(2):95-96. |
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| Authors: | Meng YanqiuZhao MingyuZhang Dayang |
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| Abstract: | N,N-diethyl-o-ethylaniline was synthesized by using benzyl triethylammonium chloride as a phase
transfer catalyst under normal atmosphere. The optimum parameters for preparing
N,N-diethyl-o-ethylaniline have been studied. |
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| Keywords: | N N-Diethyl-o-ethylaniline Synthesis Alkylation |
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