| 人尿中克罗帕米的GC/MSD检测方法研究 |
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| 引用本文： | 秦旸,朱绍棠,徐友宣. 人尿中克罗帕米的GC/MSD检测方法研究[J]. 质谱学报, 2001, 22(1): 21-21 |
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| 作者姓名： | 秦旸 朱绍棠 徐友宣 |
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| 作者单位： | 国家体育总局运动医学研究所兴奋剂检测中心, |
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| 摘 要： | 建立了人尿中克罗帕米的GC/MSD的检测方法 ,发现了三种甲基化产物。比较了不同的提取方法 ,碱性提取收率可达 94 5 %。研究了克罗帕米在人尿中的排泄情况
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| 关 键 词： | 克罗帕米 GC/MSD 检测 |
| 收稿时间： | 2000-05-30 |
| 修稿时间： | 2000-05-30 |
Determination of Clopamide in Human Urine by GC/MSD |
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| QIN Yang,Zhu Shaotang,Xu Youxuan. Determination of Clopamide in Human Urine by GC/MSD[J]. Journal of Chinese Mass Spectrometry Society, 2001, 22(1): 21-21 |
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| Authors: | QIN Yang Zhu Shaotang Xu Youxuan |
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| Abstract: | Clopamide as a new diuretic was forbidden by IOC.A new reliable GC/MSD determination method of clopamide in human urine is described in this paper.Three methyled compounds are found and varieties of extraction procedures are compared.The basic extraction recovery is 94.5%. The excretion profile of clopamide in human urine has been investigated.Clopamide could be detected in human urine within 20 hours. |
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| Keywords: | clopamide determination GC/MSD |
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