| 732阳离子交换树脂催化合成己二酸二乙酯 |
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| 引用本文： | 刘凯,魏海英,李航舵,张英杰,刘东升.732阳离子交换树脂催化合成己二酸二乙酯[J].广州化工,2011,39(15):86-88. |
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| 作者姓名： | 刘凯 魏海英 李航舵 张英杰 刘东升 |
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| 作者单位： | 1. 河北大学化学与环境科学学院,河北保定,071002
2. 空军驻杭州地区军事代表室,浙江杭州,311232 |
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| 摘 要： | 应用732阳离子交换树脂作为催化剂合成己二酸二乙酯,探讨了不同因素对于己二酸二乙酯产率的影响。通过正交试验优化了反应条件。试验结果表明：酸醇摩尔比为1∶6,催化剂用量为酸质量分数的35%,反应时间为12 h,带水剂甲苯用量为25 mL,己二酸二乙酯产率为81.13%。
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| 关 键 词： | 732阳离子交换树脂 己二酸二乙酯 正交试验 |
Study on Catalytic Synthesis of Diethyl Adipate with Cation Exchange Resin 732 |
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| LIU Kai,WEI Hai-ying,LI Hang-duo,ZHANG Ying-jie,LIU Dong-sheng.Study on Catalytic Synthesis of Diethyl Adipate with Cation Exchange Resin 732[J].GuangZhou Chemical Industry and Technology,2011,39(15):86-88. |
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| Authors: | LIU Kai WEI Hai-ying LI Hang-duo ZHANG Ying-jie LIU Dong-sheng |
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| Affiliation: | 1(1 College of Chemistry and Environmental Science,Hebei University,Hebei Baoding 071002;2 Air Force Military Representative Office in Hangzhou Area,Zhejiang Hangzhou 311232,China) |
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| Abstract: | The catalytic synthesis of diethyl adipate with cation exchange resin 732 was researched.The effect factors were investigated,and the optimum experimental conditions were optimized by orthogonal experiment.The results showed that the yield of diethyl adip |
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| Keywords: | cation exchange resin 732 orthogonal test diethyl adipate |
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