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On the accurate calibration of an electrochemical oxygen meter in the 10−7 bar range
Authors:C. M. Mari  S. Pizzini  T. A. Giorgi  L. Rosai  M. Borghi
Affiliation:(1) Electrochemistry Institute, University of Milan, Via G. Venezian 21, Milano, Italy;(2) S.A.E.S. Getters S.p.A., Via Gallarate 215, 20151 Milano, Italy;(3) Present address: Inorganic Materials Dept., Instituto Donegani, Novara, Italy
Abstract:A method for the accurate standardization of an electrochemical oxygen meter, in the 10–6-10–7 bar range is described. The method is based on the use of an electrochemical oxygen leak and a chemical getter pump. In this manner problems connected with traces of hydrogen, originating from the pyrolysis of water, and traces of oxygen of unknown origin are overcome.
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