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阻燃聚氨酯软质泡沫塑料中氯含量的测定
引用本文:张亚博,Wang Zhaohua,苏正良,Zhang Peng.阻燃聚氨酯软质泡沫塑料中氯含量的测定[J].塑料科技,2008,36(8).
作者姓名:张亚博  Wang Zhaohua  苏正良  Zhang Peng
作者单位:四川理工学院材料与化学工程系,四川自贡,643000
基金项目:国家自然科学基金资助项目
摘    要:叙述了阻燃聚氨酯软质泡沫塑料中氯含量的测定方法:在助燃剂存在下,氧瓶燃烧使聚氨酯软质泡沫塑料中的有机氯转化为HCl,用稀NaOH吸收,使用硫氰酸汞分光光度法测定聚氨酯软质泡沫塑料中阻燃剂的氯含量。该方法简单快捷、精确度高,回收率为99.64%~102.41%。

关 键 词:聚氨酯  软质泡沫塑料  阻燃剂  分光光度法

Determination of Chlorine Content In Flexible Foams of Flame- retarding Polyurethane
Zhang Yabo,Wang Zhaohua,Su Zhengliang,Zhang Peng.Determination of Chlorine Content In Flexible Foams of Flame- retarding Polyurethane[J].Plastics Science and Technology,2008,36(8).
Authors:Zhang Yabo  Wang Zhaohua  Su Zhengliang  Zhang Peng
Abstract:The determination method of chlorine content in flexible foams of flame-retarding polyurethane (PU)was discussed:organic chlorine in flexible foams turned into hydrogen chloride by burning the sample with combustion adjuvant in oxygen flask,absorbed hydrogen chloride by NaOH, then the chlorine content in flexible foams of PU could be determined by mercuric thiocyanate spectrophotometric method.The determination method is easy and accurate,the recovery ratio is up to 99.64%~102.41%.
Keywords:Polyurethane  Flexible foams  Flame retardant  Spectrophotometric method
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