| 相转移催化氧化法合成对硝基苯甲酸的研究 |
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| 引用本文： | 姚蒙正,夏少青.相转移催化氧化法合成对硝基苯甲酸的研究[J].精细石油化工,1992(3):31-35. |
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| 作者姓名： | 姚蒙正 夏少青 |
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| 作者单位： | 大连理工大学精细化工系，济南炼油厂聚丙烯分厂 |
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| 摘 要： | 考察了RuO_4相转移催化氧化法合成对硝基苯甲酸的各种影响因素。讨论了次氯酸钠纯度对氧化反应的影响。在优化条件下对硝基苯甲酸的收率为87.3％,产品纯度为99％。
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| 关 键 词： | 对硝基苯甲酸 四氧化钌 次氯酸钠 相转移催化 氧化 |
A STUDY ON PREPARATION OF p-NITROBENZOIC ACID BY PHASE TRANSFER CATALYTIC OXIDATION |
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| Yao Mengzheng.A STUDY ON PREPARATION OF p-NITROBENZOIC ACID BY PHASE TRANSFER CATALYTIC OXIDATION[J].Speciality Petrochemicals,1992(3):31-35. |
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| Authors: | Yao Mengzheng |
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| Abstract: | Various factors affecting the preparation of p-nitrobenzoic acid by PTC-RuO_4-NaClO method were investigated. The influence of NaClO purity to the oxidation reaction was discussed. The yield of p-nitrobenzoic acid under optimized conditions is 87.3%. The purity of the product is 99%. |
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| Keywords: | p-nitrobenzoic acid Ruthenium Tetraoxide Sodium Hypochlorite Phase Transfer Catalysis Oxidation |
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