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高分辨NH3光谱检测的气压控制系统设计
引用本文:李梦琪,张玉钧,何莹,尤坤,王立明. 高分辨NH3光谱检测的气压控制系统设计[J]. 电子测量技术, 2021, 44(2): 36-42
作者姓名:李梦琪  张玉钧  何莹  尤坤  王立明
作者单位:中国科学院环境光学与技术重点实验室 合肥230031;中国科学院合肥物质科学研究院 合肥230031;中国科学技术大学 合肥230026;中国科学院环境光学与技术重点实验室 合肥230031;中国科学院合肥物质科学研究院 合肥230031
基金项目:国家自然科学基金青年项目(41805124);安徽省重点研究和开发计划(201904a07020093);中科院科研仪器设备研制项目(YJKYYQ20190051)资助。
摘    要:基于伯努利原理设计了被测氨气气压闭环反馈控制系统,研究了低压条件下NH3高分辨光谱特性.系统以被测氨气吸收池压力为控制对象,采用CDG800压力传感器测量吸收池气压,1路VT317电磁阀控制高压标准浓度氨气源增大吸收池中的气压,1路VT317电磁阀控制真空泵抽取吸收池的气体降低气压,构成了NH3光谱检测的低压气路;并设...

关 键 词:氨气  低压控制  线强  重叠光谱

Design of air pressure control system for high resolution NH3 spectrum detection
Li Mengqi,Zhang Yujun,He Ying,You Kun,Wang Liming. Design of air pressure control system for high resolution NH3 spectrum detection[J]. Electronic Measurement Technology, 2021, 44(2): 36-42
Authors:Li Mengqi  Zhang Yujun  He Ying  You Kun  Wang Liming
Affiliation:(Key Laboratory of Environmental Optics Technology,Chinese Academy of Sciences,Hefei 230031,China;Hefei Institute of Material Science,Chinese Academy of Sciences,Hefei 230031,China;University of Science and Technology of China,Hefei 230026,China)
Abstract:In this paper, a closed-loop feedback control system for the measured ammonia gas pressure is designed based on Bernoulli′s principle, and the high-resolution spectral characteristics of NH3 under low pressure conditions are studied. The system takes the measured ammonia absorption tank pressure as the control object, uses CDG800 pressure sensor to measure the absorption tank air pressure, one of the VT317 solenoid valve controls the high pressure standard concentration ammonia source to increase the air pressure in the absorption tank, and the other VT317 solenoid valve controls the vacuum pump extraction. The gas in the absorption cell reduces the pressure to form a low-pressure gas circuit for NH3 spectrum detection, and a closed-loop feedback control circuit for pressure measurement, solenoid valve and vacuum pump with Arduino UNO microcontroller as the core is designed. The experimental results show that the designed air pressure control system can maintain a stable time for more than 72 h, and the air pressure fluctuates within 1 torr. When the pressure is 3.2 torr, six single absorption spectrum signal in the NH3 mid-infrared band 1 103.4 cm-1 is obtained, and the deriation between the calculated line intensity and the line intensity data in the HITRAN database is between 2.71% and 4.71%, which achieves complete separation of overlapping spectral lines, which provides valuable experience for subsequent high resolution spectrum research.
Keywords:ammonia  low pressure control  line strength  overlapping spectrum
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