Fabrication of Transparent Hydroxyapatite Sintered Body with High Crystal Orientation by Pulse Electric Current Sintering |
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Authors: | Yujiro Watanabe Toshiyuki Ikoma Akira Monkawa Yasushi Suetsugu Hirohisa Yamada Junzo Tanaka Yusuke Moriyoshi |
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Affiliation: | National Institute for Materials Science, Tsukuba, Ibaraki 305-0044, Japan; Faculty of Engineering, Hosei University, Koganei, Tokyo 184-8584, Japan |
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Abstract: | Transparent hydroxyapatite (HAp) sintered body with a high crystal orientation and a relative density of 99.7% was fabricated by the pulse electric current sintering method; the c -axis of HAp crystals with a hexagonal column morphology and ca. 200 μm × 25 μm in size was oriented perpendicular to the pressure direction. The sintered temperature increased to 1200°C at a heating rate of 50°C/min for 10 min and a pressure of 50 MPa was applied. The orientation indexes were calculated from X-ray diffraction patterns of the planes perpendicular and parallel to the pressure direction. The optical transmittance was greater than 70% over the wavelength of 700 nm. |
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