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合成样品中3-甲氧基四氟丙酸甲酯的测定
引用本文:陈章跃,雷迅,戴宏文,陈晓莉. 合成样品中3-甲氧基四氟丙酸甲酯的测定[J]. 云南化工, 2011, 38(2): 25-27
作者姓名:陈章跃  雷迅  戴宏文  陈晓莉
作者单位:1. 宁波市北仑区环境监测站,浙江,宁波,315800
2. 浙江巨化集团技术中心,浙江,衢州,324004
摘    要:研究了测定合成样品中3-甲氧基四氟丙酸甲酯含量的方法,采用毛细管气相色谱法,以环氧氯丙烷为内标物,分析合成样品中的两种目的组分,结果表明,该法准确可靠,标准偏差0.23%,变异系数0.94%,可用于该合成样品的定量分析。

关 键 词:3-甲氧基四氟丙酸甲酯  毛细管气相色谱法  环氧氯丙烷

Dertermination of 3-Methoxy Tetrafluoropropionic Acid Methyl Ester in Synthetic Samples
CHEN Zhang-yue,LEI Xun,DAI Hong-wen,CHEN Xiao-li. Dertermination of 3-Methoxy Tetrafluoropropionic Acid Methyl Ester in Synthetic Samples[J]. Yunnan Chemical Technology, 2011, 38(2): 25-27
Authors:CHEN Zhang-yue  LEI Xun  DAI Hong-wen  CHEN Xiao-li
Affiliation:CHEN Zhang-yue1,LEI Xun1,DAI Hong-wen2,CHEN Xiao-li2 (1.Beilun Environmental Monitoring Station,Ningbo Zhejiang 315800,China,2.Technology Center of Juhua Group,Quzhou 324004,China)
Abstract:Study on the determination method of 3-Methoxy tetrafluoropropionic acid methyl ester in the synthesis samples by CGC method,using Epichlorohydrin as internal standard,two kinds of purposed constituents in synthetic samples could be determined.Experimental results showed that this method is accurate,the standard deviation is 0.23%,coefficient of variation is 0.94%,so it can be applied to quantitative analysis for the synthetic samples.
Keywords:3-methoxytetrafluoropropionic acid methyl ester  CGC  epichlorohydrin  
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