| 微波辐射下3-(N,N-二羧甲基)氨甲基水杨酸的合成 |
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| 引用本文： | 刘庆,陈刚,魏俊发,刘玲,吴亚,乔珍,黄涛,邓芳. 微波辐射下3-(N,N-二羧甲基)氨甲基水杨酸的合成[J]. 化学与生物工程, 2005, 22(5): 37-38 |
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| 作者姓名： | 刘庆 陈刚 魏俊发 刘玲 吴亚 乔珍 黄涛 邓芳 |
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| 作者单位： | 陕西师范大学化学与材料科学学院,陕西,西安,710062;中国科学院昆明植物研究所,云南,昆明,650204 |
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| 摘 要： | 常规法合成3-(N，N-二羧甲基)氨甲基水杨酸需要在水溶液中长时间加热制备，作者用微波辐射合成了3-(N，N-二羧甲基)氨甲基水杨酸。结果较理想，与常规方法相比，反应时间缩短了14倍且产率达61％。
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| 关 键 词： | 微波辐射 合成 Mannich反应 |
| 文章编号： | 1672-5425(2005)05-0037-02 |
| 修稿时间： | 2005-03-07 |
Synthesis of 3-[N, N-Bis (2-acetoxy) Aminomethyl] Salicylic under Microwave Irradiation |
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| LIU Qing,CHEN Gang,WEI Jun-fa,LIU Ling,Wu YA,QIAO Zhen,HUANG Tao,DENG Fang. Synthesis of 3-[N, N-Bis (2-acetoxy) Aminomethyl] Salicylic under Microwave Irradiation[J]. Chemistry & Bioengineering, 2005, 22(5): 37-38 |
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| Authors: | LIU Qing CHEN Gang WEI Jun-fa LIU Ling Wu YA QIAO Zhen HUANG Tao DENG Fang |
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| Abstract: | N,N-Bis (2-acetoxy) aminomethyl] salicylic was synthesized under microwave irradiation. Compared with conventional synthesis,the rate of reaction was up to 14 times faster under such condition than by conventional method,and the yield was 61%. |
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| Keywords: | microwave irradiation synthesis Mannich reaction |
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