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| 缓冲溶液沉淀法制备氧化镁稳定氧化锆纳米粉体 | |
| 引用本文： | 苏存萍,林元华,邓旭亮,胡晓阳,马琦,王勇.缓冲溶液沉淀法制备氧化镁稳定氧化锆纳米粉体[J].稀有金属材料与工程,2009,38(Z2). |
| 作者姓名： | 苏存萍 林元华 邓旭亮 胡晓阳 马琦 王勇 |
| 作者单位： | 1. 北京大学口腔医学院,北京,100081;清华大学,新型陶瓷与精细工艺国家重点实验室,北京,100084;佳木斯大学口腔医学院,黑龙江,佳木斯,154002 2. 清华大学,新型陶瓷与精细工艺国家重点实验室,北京,100084 3. 北京大学口腔医学院,北京,100081 |
| 基金项目： | 国家高技术研究发展("863")计划 |
| 摘 要： | 以ZrOCl_2·8H_2O、MgCl_2为原料,NH_3·H_2O为沉淀剂,采用缓冲溶液沉淀法制备MgO-ZrO_2前驱体粉体.通过差热分析、X射线衍射、透射电镜等对所得粉体进行测定分析.结果表明:获得了粒径10～20 nm淡黄色氧化镁稳定的氧化锆陶瓷(MgO-ZrO_2)粉体.在稳定剂浓度为10 mol/L时,可获得纯的四方相氧化锆纳米粒子,有望用于口腔齿科材料中. |
| 关 键 词： | 缓冲溶液沉淀法 稳定剂 |
Preparation of Magnesium Stabilized Zirconia Nanoparticles by Buffer Solution Precipitation |
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| Su Cunping,Lin Yuanhua,Deng Xuliang,Hu Xiaoyang,Ma Qi,Wang Yong.Preparation of Magnesium Stabilized Zirconia Nanoparticles by Buffer Solution Precipitation[J].Rare Metal Materials and Engineering,2009,38(Z2). | |
| Authors: | Su Cunping Lin Yuanhua Deng Xuliang Hu Xiaoyang Ma Qi Wang Yong |
| Affiliation: | Su Cunping1,2,3,Lin Yuanhua2,Deng Xuliang1,Hu Xiaoyang1,Ma Qi1,Wang Yong1 (1. Peking University School of Stomatology,Beijing 100081,China) (2. State key Laboratory of New Ceramics , Fine Processing,Tsinghua University,Beijing 100084,China) (3. Jiamusi University,Jiamusi 154002,China) |
| Abstract: | Nanosized MgO-ZrO_2 precursor powders were prepared by buffer-solution precipitation processing using zirconium oxychloride (ZrOCl_2·8H_2O) and magnesium chloride (MgCl_2) as the raw materials, and NH_3 ·H_2O as the precipitation agent. The synthesized powders were characterized by XRD, TEM and DSC-TG. The spherical MgO-ZrO_2 particles with an average diameter of 10～20 nm can be obtained. Phase composition analysis indicates that ZrO_2 powders are pure tetragonal phase as the concentration of stabilizer is 10 mol/L, which can be potential for dental ceramics application. |
| Keywords: | MgO-ZrO_2 buffer solution precipitation MgO-ZrO_2 stabilizer |
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