| 松香酸根插层剥离型纳米水滑石材料的制备与表征 |
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| 引用本文： | 吴燕,章文贡,高鹏举.松香酸根插层剥离型纳米水滑石材料的制备与表征[J].现代化工,2012(1):38-40,42. |
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| 作者姓名： | 吴燕 章文贡 高鹏举 |
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| 作者单位： | 福建师范大学化学与材料学院高分子研究所 |
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| 基金项目： | 福建省纳米重大专项资助项目(2005HZ01-5) |
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| 摘 要： | 采用共沉淀法制备了松香酸根插层剥离型纳米水滑石。借助红外光谱、X射线衍射、热分析和高分辨透射电镜等对其进行了表征。结果表明,随着松香酸根插入镁铝水滑石层间,水滑石层间距逐渐增大,最终克服水滑石层板间作用力而将其剥离,形成了剥离型纳米水滑石材料。该材料的热稳定性也得到显著提高,具有潜在的应用价值。
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| 关 键 词： | 松香酸根 水滑石 剥离 共沉淀法 纳米 |
Synthesis and characterization of delaminated abietate radical intercalated hydrotalcite nano material |
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| WU Yan,ZHANG Wen-gong,GAO Peng-ju.Synthesis and characterization of delaminated abietate radical intercalated hydrotalcite nano material[J].Modern Chemical Industry,2012(1):38-40,42. |
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| Authors: | WU Yan ZHANG Wen-gong GAO Peng-ju |
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| Affiliation: | (Institute of Polymer Science,College of Chemistry and Materials Science,Fujian Normal University, Fuzhou 350007,China) |
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| Abstract: | The delaminated abietate radical intercalated into the nano MgAl-abietate radical-LDH(layered double hydroxides) was synthesized using the co-precipitation method.The sample was characterized by Fourier Transform Infrared(FT-IR) spectroscopy,X-Ray Diffraction(XRD),Thermogravimetry(TG) and High Resolution Transmission Electron Microscopy(HRTEM).The results show that the interlamellar spacing of LDH increases gradually with the abietate radical intercalating into the LDH.Finally,the delaminated nano-LDH is formed when the abietate radical overcomes the force between the layers of the LDH.The thermal stability of the MgAl-abietate radical-LDH is remarkably improved,compared with that of MgAl-LDH,which makes it potential for applications. |
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| Keywords: | abietate radical LDH delamination co-precipitation method nano material |
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