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Fabrication and mechanical properties of SiC platelet reinforced mullite matrix composites
Affiliation:1. College of Chemistry and Life Sciences, Zhejiang Normal University, Jinhua 321004, People''s Republic of China;2. State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 437000, People''s Republic of China;1. College of Liberal Arts, Semyung University, Chechon, Chungbuk 27136, Republic of Korea;2. Chemical Materials Solutions Center, Korea Research Institute of Chemical Technology, Daejeon 34114, Republic of Korea;3. Department of Physics, Hallym University, Gangwondo 24252, Republic of Korea;4. Department of Nano Fusion Technology, Pusan National University, Busan 46241, Republic of Korea
Abstract:Hot-pressing of mullite and SiC–mullite matrix composites was performed at temperatures and pressures between 1500 and 1650°C and 5 and 15 MPa, respectively. Composites were produced using different precursors; sol–gel derived mullite and kaolinite/α-alumina. The precursor did not strongly affect the optimum density achieved, reaching 97·5% of theoretical for a 20 vol% SiC addition in both cases. The SiC platelet addition impaired densification kinetics in all composites compared to mullite monoliths. Fracture toughness, measured by the indentation strength in bending technique, was marginally higher for the sol–gel precursor material in both monolith and composite. Fracture toughness increased with SiC content for both materials. For example, for the sol-gel precursor material it increased from 2.9±0.1 MPa m1/2 for the monolith to 3.9±0.1 MPa m1/2 for the 20 vol% SiC composite. Similarly, hardness increased with SiC addition for both materials, but the hardness of the sol–gel material was greater than that of the kaolinite+α-alumina material for all compositions. The relationship between microstructure and mechanical properties is discussed.
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