| 无需衍生化样品处理快速测定食品中 黄曲霉毒素B1 |
| |
| 引用本文： | 雷红琴,李 芳,黎琳琳,刘绪斌,沙 力,李艳美,储晓刚,粟有志. 无需衍生化样品处理快速测定食品中 黄曲霉毒素B1[J]. 食品安全质量检测学报, 2014, 5(9): 2859-2863 |
| |
| 作者姓名： | 雷红琴 李 芳 黎琳琳 刘绪斌 沙 力 李艳美 储晓刚 粟有志 |
| |
| 作者单位： | 伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心,中国检验检疫科学研究院,伊犁出入境检验检疫局综合技术服务中心,伊犁出入境检验检疫局综合技术服务中心 |
| |
| 摘 要： | 建立无衍生-超高效液相色谱法测定食品中的黄曲霉毒素B1的快速检测方法。样品经甲醇-水提取,免疫亲和柱净化,C18色谱柱分离、大体积流通池荧光检测器检测。黄曲霉毒素B1在0.10 ng/ml~5.00 ng/ml范围内与峰面积呈良好线性关系,R2>0.999,在6种基质,0.50 μg/kg~2.00 μg/kg范围内加标,平均回收率在71.7%~111.2%之间,相对标准偏差(RSD)为3.8%~11.5%,检出限(LOD)为0.05 μg/kg。本方法灵敏、快速、无衍生、结果准确,能够满足食品中黄曲霉毒素B1残留的检测需求。
|
| 关 键 词： | 黄曲霉毒素B1 超高效液相色谱法 免疫亲和柱 无衍生 |
| 收稿时间： | 2014-07-22 |
| 修稿时间： | 2014-09-01 |
Rapid determination of aflatoxin B1 in foods without derivation |
| |
| LEI Hong-Qin,LI Fang,Li Lin-Lin,LIU Xu-Bin,Sha LI,LI Yan-Mei,CHU xiao-Gang and SU You-Zhi. Rapid determination of aflatoxin B1 in foods without derivation[J]. Journal of Food Safety & Quality, 2014, 5(9): 2859-2863 |
| |
| Authors: | LEI Hong-Qin LI Fang Li Lin-Lin LIU Xu-Bin Sha LI LI Yan-Mei CHU xiao-Gang SU You-Zhi |
| |
| Affiliation: | (Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,. Comprehensive Technical Service Center of Yili Entry-Exit Inspection and Quarantine Bureau,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,Chinese Academy of Inspection and Quarantine,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau,(Comprehensive Technical Service Center complex laboratory of Yi Li Exit-Entry Inspection and Quarantine Bureau |
| |
| Abstract: | |
| |
| Keywords: | Aflatoxin B1 Ultra performance liquid chromatography Immuno-affinity column Without derivation |
|
| 点击此处可从《食品安全质量检测学报》浏览原始摘要信息 |
|
点击此处可从《食品安全质量检测学报》下载全文 |
|
