| 原子吸收分光光度法测定连翘提取液中重金属含量 |
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| 引用本文： | 欧阳玉祝,旷超阳,田守飞,张辞海.原子吸收分光光度法测定连翘提取液中重金属含量[J].应用化工,2011,40(8). |
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| 作者姓名： | 欧阳玉祝 旷超阳 田守飞 张辞海 |
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| 作者单位： | 吉首大学化学化工学院,湖南 吉首,416000 |
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| 基金项目： | 湖南省科技厅科技计划项目(2008FJ3077); 湖南省大学生创新性实验计划项目(湘教通〔2011〕272号) |
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| 摘 要： | 以连翘为原料,用火焰原子吸收分光光度法测定了连翘提取液中铅、铬、镉、铜、锌含量。实验结果表明,连翘中铅、铬、镉、铜、锌含量依次为0.78,0.55,0.09,13.31,38.86μg/g,平均加标回收率为99.72%,97.02%,98.50%,99.81%,99.51%。精密度和重复性分析的RSD分别为3.47%,2.83%,4.21%,1.03%,0.52%和1.26%,1.77%,4.07%,0.19%,0.10%。
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| 关 键 词： | 连翘 原子吸收分光光度法 重金属 |
Determination of heavy metal content in forsythia by FAAS |
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| OUYANG Yu-zhu,KUANG Chao-yang,TIAN Shou-fei,ZHANG Ci-hai.Determination of heavy metal content in forsythia by FAAS[J].Applied chemical industry,2011,40(8). |
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| Authors: | OUYANG Yu-zhu KUANG Chao-yang TIAN Shou-fei ZHANG Ci-hai |
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| Affiliation: | OUYANG Yu-zhu,KUANG Chao-yang,TIAN Shou-fei,ZHANG Ci-hai(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,China) |
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| Abstract: | With forsythia as raw materials,content of lead,chromium,cadmium,copper and zinc in forsythia extracts was analysed by flame atomic absorption spectrophotometry.The results showed that contents of plumbum,chromium,cadmium,copper and zinc in forsythia were 0.78,0.55,0.09,13.31,38.86 μg/g,and average recovery rate of adding standard sample were 99.72%,97.02%,98.50%,99.81%,99.51%.RSD of precision and repeatability analysis were 3.47%,2.83%,4.21%,1.03%,0.52% and 1.26%,1.77%,4.07%,0.19%,0.10%,respectively. |
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| Keywords: | forsythia atomic absorption spectrophotometry heavy metal |
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