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茜草总黄酮提取工艺研究
引用本文:田春莲,蒋凤开.茜草总黄酮提取工艺研究[J].食品科学,2011(24).
作者姓名:田春莲  蒋凤开
作者单位:吉首大学林产化工工程湖南省重点实验室;吉首大学生物资源与环境科学学院;
基金项目:湖南省科技计划项目(2010TP4007-1); 林产化工工程湖南省重点实验室开放基金项目(JDZ200906); 湖南省高校“林产资源化学与林化产品开发”科技创新团队支持计划项目(湘教通(2010)212号)
摘    要:研究茜草总黄酮的提取工艺条件。采用热浸提法提取茜草总黄酮,硝酸铝显色法测定总黄酮提取率。通过单因素试验研究乙醇体积分数、料液比、提取温度、提取时间对黄酮提取率的影响,通过正交试验进一步优化提取工艺条件。单因素试验结果显示,乙醇体积分数50%、提取温度70℃、提取时间2.5h、料液比1:40(g/mL)条件下茜草总黄酮提取率较高;正交试验结果表明:茜草总黄酮的最佳提取工艺为60%、乙醇溶液提取2h、提取温度70℃、料液比1:40(g/mL),此条件下茜草总黄酮提取率为1.67%。本工艺简单可行,有较好的参考价值。

关 键 词:茜草  总黄酮  提取工艺  

Optimization of Extraction Process for Total Flavonoids from Madder Root
TIAN Chun-lian,JIANG Feng-kai.Optimization of Extraction Process for Total Flavonoids from Madder Root[J].Food Science,2011(24).
Authors:TIAN Chun-lian  JIANG Feng-kai
Affiliation:TIAN Chun-lian1,JIANG Feng-kai2 (1.Key Laboratory of Hunan Forest Products and Chemical Industry Engineering,Jishou University,Zhangjiajie 427000,China,2.College of Biology and Environmental Sciences,Jishou 416000,China)
Abstract:This study was carried out to optimize the hot water extraction of total flavonoids from madder root.The effects of 4 process parameters including ethanol concentration,material-to-liquid ratio,temperature and extraction duration on extraction efficiencywere investigated by one-factor-at-a-time method and orthogonal array design.The results form the one-factor-at-a-time experiments showed that the optimal extraction conditions were 50% aqueous ethanol as extraction solvent at a material-to-liquid ratio of 1...
Keywords:madder  total flavanoids  extraction  
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