| 一种咪唑啉季铵盐的合成 |
| |
| 引用本文： | 孟邱,张宇,闫慧,黄玮,丛玉凤.一种咪唑啉季铵盐的合成[J].应用化工,2011,40(8):1416-1417,1420. |
| |
| 作者姓名： | 孟邱 张宇 闫慧 黄玮 丛玉凤 |
| |
| 作者单位： | 辽宁石油化工大学石油化工学院,辽宁 抚顺,113001 |
| |
| 摘 要： | 以硬脂酸和二乙烯三胺为原料,经酰胺化和环化脱水合成硬脂酸咪唑啉中间体,再加入乙醇和乙酸使之转化为水溶性的咪唑啉季铵盐。研究表明,合成硬脂酸咪唑啉季铵盐的最佳工艺条件为:酸胺摩尔比为1∶1,环化反应温度为210℃,环化反应时间为5 h。
|
| 关 键 词： | 缓蚀剂 咪唑啉 硬脂酸 挂片失重法 |
Synthesis of an imidazolium quaterary |
| |
| MENG Qiu,ZHANG Yu,YAN Hui,HUANG Wei,CONG Yu-feng.Synthesis of an imidazolium quaterary[J].Applied chemical industry,2011,40(8):1416-1417,1420. |
| |
| Authors: | MENG Qiu ZHANG Yu YAN Hui HUANG Wei CONG Yu-feng |
| |
| Affiliation: | MENG Qiu,ZHANG Yu,YAN Hui,HUANG Wei,CONG Yu-feng(Department of Petrochemical Engineering,Liaoning University of Petroleum & Chemical Technology,Fushun 113001,China) |
| |
| Abstract: | With stearic acid and diethylenetriamine as raw materials,stearic imidazoline intermediate was synthesized by amidation and cyclization.It transformed into water-soluble imidazolium quaternary after adding the ethanol and acetic acid.The results showed that optimum conditions of synthesis of stearic acid imidazoline intermediates was that molar ratio of acid to amine 1∶1,reaction temperature of cyclization 210 ℃ and reaction time of cyclization 5 h. |
| |
| Keywords: | corrosion inhibitor imidazoline stearic acid methods of coupon weight loss |
| 本文献已被 CNKI 万方数据 等数据库收录！ |
|
