| Synthesis of ZnO doped ceria nanoparticles via azeotropic distillation processing |
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| 引用本文： | 宋晓岚 曲鹏 杨华明 邱冠周. Synthesis of ZnO doped ceria nanoparticles via azeotropic distillation processing[J]. 中国有色金属学会会刊, 2006, 16(B01): 350-355. DOI: 10.1016/S1003-6326(06)60208-2 |
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| 作者姓名： | 宋晓岚 曲鹏 杨华明 邱冠周 |
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| 作者单位： | School of Resources Processing and Bioengineering, Central South University, Changsha 410083, China |
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| 基金项目： | Project （2005DFBA028） supported by the International Cooperation of Science and Technology Ministry of PRC; Project （59925412） supported by the National Natural Science Foundation of China |
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| 摘 要： | The synthesis of nano-sized ZnO-doped CeO2 of 20 nm in crystal size by a coprecipitation technique was investigated by different scanning calorimetries/thermalgravimetrics（DSC/TG）, X-ray diffraction （XRD）, transmission electron microscopy （TEM） and ultraviolet （UV） absorbance. Azeotropic distillation processing was performed to effectively eliminate the residual water inside the as-prepared precipitate. Doping of ZnO results in the formation of solid solution. The crystal size of the nanoparticles increases with the increase of the doped ZnO amount, the calcination temperature and time. Doped CeO2 nanoparticles show excellent visible-light property and ultraviolet-absorption activity. Doping of ZnO doesn＇t not weaken the UV-shielding property of ceria.
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| 关 键 词： | 氧化锌掺杂 二氧化铈纳米粒子 合成 共沸蒸馏工艺 紫外吸光率 遮光剂 |
| 收稿时间： | 2006-04-10 |
| 修稿时间： | 2006-04-25 |
Synthesis of ZnO doped ceria nanoparticles via azeotropic distillation processing |
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| SONG Xiao-lan, QU Peng, YANG Hua-ming, QIU Guan-zhou. Synthesis of ZnO doped ceria nanoparticles via azeotropic distillation processing[J]. Transactions of Nonferrous Metals Society of China, 2006, 16(B01): 350-355. DOI: 10.1016/S1003-6326(06)60208-2 |
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| Authors: | SONG Xiao-lan QU Peng YANG Hua-ming QIU Guan-zhou |
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| Affiliation: | 1. Laboratoire de chimie physique, Département de chimie, Faculté des Sciences de Sfax, Université de Sfax, Tunisia;2. Département de Mathématiques, Faculté des Sciences, Université de Sfax, Sfax, Tunisia;3. Department of Civil, Chemical and Environmental Engineering, University of Genoa, P.le J.F. Kennedy 1, 16129 Genoa, Italy |
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| Abstract: | The synthesis of nano-sized ZnO-doped CeO2 of 20 nm in crystal size by a coprecipitation technique was investigated by different scanning calorimetries/thermalgravimetrics(DSC/TG), X-ray diffraction (XRD), transmission electron microscopy (TEM) and ultraviolet (UV) absorbance. Azeotropic distillation processing was performed to effectively eliminate the residual water inside the as-prepared precipitate. Doping of ZnO results in the formation of solid solution. The crystal size of the nanoparticles increases with the increase of the doped ZnO amount, the calcination temperature and time. Doped CeO2 nanoparticles show excellent visible-light property and ultraviolet-absorption activity. Doping of ZnO doesn't not weaken the UV-shielding property of ceria. |
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| Keywords: | ceria nanoparticles ZnO doping inorganic compounds nanostructures oxides |
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