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Deposition of AlN films by reactive sputtering: Effect of radiofrequency substrate bias
Authors:B. Abdallah  A. Chala  M.P. Besland  M.A. Djouadi
Affiliation:a Institut des Matériaux Jean Rouxel IMN UMR 6502, Université de Nantes, 2 rue de La Houssinière BP 32229, 44322 Nantes Cedex France
b IUT MPh, Université de Valenciennes et du Hainaut-Cambrésis, Zone Industrielle du Champ de l’Abbesse, 59600 Maubeuge, France
c Département de Physique, Université de Biskra, BP 145 RP, 07000 Biskra, Algeria
d Atomic Energy Commission Syrian (AECS), BP 6091, Damascus, Syrian Arab Republic
Abstract:Piezoelectric AlN thin films were deposited on Silicon substrates by triode reactive sputtering. The variation of residual stress versus bias voltage on the substrate was investigated. A compressive stress was always observed with a maximum value for a negative substrate bias of 50 V. For higher negative bias voltage values, the compressive stress decreases. X-ray diffraction measurements showed two kinds of growth orientation. First, without bias voltage, films are well crystallized and (002) oriented. Second, with bias voltage, the (002) orientation disappears and a small peak appears (situated in the 2θ = 32°-33° range) which can be attributed to (100) orientation. Finally, the influence of compressive stress and ion bombardment on the change of orientation is discussed.
Keywords:Aluminium nitride   X-ray diffraction   stress measurements   substrate bias effect
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