Synthesis of mesoporous molecular sieves: influence of aluminum source on Al incorporation in MCM-41 |
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| Authors: | Kondam Madhusudan Reddy Chunshan Song |
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| Affiliation: | (1) Fuel Science Program, Department of Material Science and Engineering, The Pennsylvania State University, 16802 University Park, PA, USA |
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| Abstract: | Three series of mesoporous aluminosilicate molecular sieves, MCM-41, with various Si/Al ratios were synthesized using different aluminum sources (aluminum isopropoxide, pseudo boehmite and aluminum sulfate). XRD analysis, temperature programmed desorption ofn-butylamine,27Al and29Si MAS NMR, and catalytic alkylation test indicated that aluminum isopropoxide is a better source for incorporating aluminum in the framework of MCM-41 type molecular sieves with better crystallinity and acid characteristics. |
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| Keywords: | mesoporous materials MCM-41 synthesis aluminum source |
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