| 高纯度四碱式硫酸铅的制备 |
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| 引用本文： | 吴战宇,雷立旭,顾立贞,董志成,张琳. 高纯度四碱式硫酸铅的制备[J]. 电池工业, 2011, 16(2): 83-85 |
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| 作者姓名： | 吴战宇 雷立旭 顾立贞 董志成 张琳 |
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| 作者单位： | 吴战宇,董志成,张琳,WU Zhan-yu,DONG Zhi-cheng,ZHANG Lin(江苏华富控股集团有限公司,江苏扬州,225600);雷立旭,LEI Li-xu(东南大学化学化工学院,江苏南京,211106);顾立贞,GU Li-zhen(江苏华富控股集团有限公司,江苏扬州225600;东南大学化学化工学院,江苏南京211106) |
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| 摘 要： | 以烧结法为基础,制备了高纯度四碱式硫酸铅材料;利用XRD对四碱式硫酸铅产品成分进行分析检测,系统考察了反应物配比、反应温度和反应时间对产物中四碱式硫酸铅含量的影响;实验结果表明:以氧化铅为主要原料,同时在反应物料中加入少量硫酸铅,与硫酸反应后进行烧结,产物中四碱式硫酸铅含量最高,可以达到99%。
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| 关 键 词： | 铅蓄电池 四碱式硫酸铅 烧结 高纯度 |
Preparation of high purity tetrabasic lead sulphate |
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| WU Zhan-yu,LEI Li-xu,GU Li-zhen,DONG Zhi-cheng,ZHANG Lin. Preparation of high purity tetrabasic lead sulphate[J]. Chinese Battery Industry, 2011, 16(2): 83-85 |
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| Authors: | WU Zhan-yu LEI Li-xu GU Li-zhen DONG Zhi-cheng ZHANG Lin |
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| Affiliation: | WU Zhan-yu1,LEI Li-xu2,GU Li-zhen1,3,DONG Zhi-cheng1,ZHANG Lin1(1.Jiangsu Huafu Holding Group Co.,Ltd.,Yangzhou,Jiangsu 225600,China,2.School of Chemistry and Chemical Engineering,Southeast University,Nanjing,Jiangsu 211106,3.Jiangsu Huafu Power Storage New Technology Development Co.,China) |
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| Abstract: | Based on sintering method,the high purity tetrabasic lead sulphate was prepared in this paper.And its purity was tested by XRD,and the reactant ratios,reaction temperature and reaction time were detected to indicate their influences on the purity of tetrabasic lead sulphate.The experiment results showed that,the optimum conditions of preparing high purity tetrabasic lead sulphate were mixing lead oxide with a part of lead sulfate and sintering the reactant after reacting with sulfuric acid,and the highest c... |
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| Keywords: | lead-acid battery tetrabasic lead sulphate sintering high purity |
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