| 三氯生合成的研究(Ⅱ) |
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| 引用本文： | 宋健,冯荣秀,李效军,陈磊,王琨,石巍,王军波.三氯生合成的研究(Ⅱ)[J].化学工业与工程,2002,19(4):301-304,F003. |
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| 作者姓名： | 宋健 冯荣秀 李效军 陈磊 王琨 石巍 王军波 |
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| 作者单位： | 天津大学药物科学与技术学院,天津,300072 |
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| 摘 要： | 三氯生是一种优异的杀菌添加剂，广泛用于卫生保健等领域。其合成一般是以2，4－二氯苯酚和2，5－二氯硝基苯为原料，经过醚化、硝基还原、重氮化、水解等几步反应。本文研究了重氮化、水解两步反应及其影响因素。
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| 关 键 词： | 三氯生 合成 研究 2 4 4‘－三氯－2’－氨基－二苯醚 2 4 4‘－三氯－2’－羟基－二苯醛 重氮化 水解 |
| 文章编号： | 1004-9533(2002)04-0301-04 |
Study on the Synthesis of Triclosan(Ⅱ) |
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| SONG Jian,FENG Rong xiu,LI Xiao jun,CHEN Lei,WANG Kun,SHI Wei,WANG Jun bo.Study on the Synthesis of Triclosan(Ⅱ)[J].Chemical Industry and Engineering,2002,19(4):301-304,F003. |
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| Authors: | SONG Jian FENG Rong xiu LI Xiao jun CHEN Lei WANG Kun SHI Wei WANG Jun bo |
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| Abstract: | Triclosan is a kind of bactericides that has found applications in hygiene and health.Synthesis of triclosan from 2,4 Dichlorophenol and 2,5 Dichloro nitrobenzene usually involves such procedure as etherization,reduction of nitro group,diazotization and hydrolysis.The last two steps were studied in this paper. |
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