| 反-反-2,4-己二烯醇高效液相色谱分析方法研究 |
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| 引用本文： | 丁白瑜,江忠萍. 反-反-2,4-己二烯醇高效液相色谱分析方法研究[J]. 山东化工, 2014, 0(2): 57-59 |
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| 作者姓名： | 丁白瑜 江忠萍 |
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| 作者单位： | [1]山东省化学农药重点实验室山东省农药研究所,山东济南250033 [2]山东大学晶体材料国家重点实验室,山东济南250100 |
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| 摘 要： | 本文建立了一种用高效液相色谱测定反式-反式-2,4-己二烯醇的定量分析方法。它采用Inertsil ODS-SP C18色谱柱,以甲醇-磷酸水溶液(体积比为60∶40)为流动相,流量为1.0 mL/min,柱温为30°C,选择230 nm为检测波长进行检测。结果显示该方法的线性相关系数0.9990,标准偏差为0.092,平均回收率为100.2%。此方法简便、快速、能进行准确定量分析,结果稳定。
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| 关 键 词： | 反-反-2,4-己二烯醇 高效液相色谱 分析 |
Determination of trans,trans-2, 4-Hexadien-1-ol by HPLC |
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| Affiliation: | DING Bai - yu, JIANG Zhong -ping ( 1. Shandong Province Key Laboratory of Chemical Pesticide, Shandong Pesticide Research Institute, Jinan 250033, China; 2. State Key Laboratory of Crystal Materials, Shandong University, Jinan 250100, China) |
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| Abstract: | [ Aims ] A HPLC method was developed for the quantitative determination of trans, trans - 2, 4 - Hexadien - 1 -ol. [Methods]The mobile phase was a 60：40 mixture of methanol and water, flow rate was 1.0 mL/min, and a C18 chromatographic column was used with column temperature at 30 ℃ and the detection wave length was 230 nm. [ Results ] The linear correlation coefficient was 0. 9990, the standard deviation was 0.092, and the average recovery was 100.2 %. [ Conclusions ] The method has the advantages of convenience, fast speed, accurate quantitative analysis, and the results are stable. |
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| Keywords: | trans, trans - 2, 4 - Hexadien - 1 - ol HPLC analysis |
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