| 用气相色谱法定量分析川芎挥发油的化学成分 |
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| 引用本文： | 姚二民,张峻松,王花俊,谭宏祥.用气相色谱法定量分析川芎挥发油的化学成分[J].日用化学工业,2006,36(5):328-330. |
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| 作者姓名： | 姚二民 张峻松 王花俊 谭宏祥 |
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| 作者单位： | 1. 郑州轻工业学院,食品生物工程学院,河南,郑州,450002
2. 张家口卷烟厂,河北,张家口,075000 |
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| 基金项目： | 河南省骨干教师资助项目(04024) |
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| 摘 要： | 采用超临界流体萃取得到川芎挥发油,平均出油率为6.64%。利用毛细管气相色谱仪对川芎挥发油的16种化学成分进行了定量分析;回归方程的相关系数为0.995 1~0.999 8;回收率在83.82%~96.74%,RSD在1.68%~4.18%。该方法快速、简便、准确,适于川芎挥发油的主要化学成分分析。
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| 关 键 词： | 香料 川芎挥发油 定量分析 |
| 文章编号： | 1001-1803(2006)05-0328-03 |
| 收稿时间： | 05 15 2006 12:00AM |
| 修稿时间： | 06 12 2006 12:00AM |
Quantitative analysis of chemical compounds of volatile oil in Ligusticum Chuanxiong Hort by gas chromatography |
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| YAO Er-min,ZHANG Jun-song,WANG Hua-jun,TAN Hong-xiang.Quantitative analysis of chemical compounds of volatile oil in Ligusticum Chuanxiong Hort by gas chromatography[J].China Surfactant Detergent & Cosmetics,2006,36(5):328-330. |
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| Authors: | YAO Er-min ZHANG Jun-song WANG Hua-jun TAN Hong-xiang |
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| Affiliation: | 1. School of Food and Bioengineering, Zhengzhou Institute of Light Indnstry,Zhengzhou 450002, China; 2.Zhangjiakou Cigarette Factory, Zhangjiakou 833200, China |
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| Abstract: | The volatile oil of Ligusticum Chuanxiong Hort was prepared by supercritical fluid extraction.The average yield is 6.64%.The quantitative analyses of 16 chemical compounds were conducted by capillary GC method.The recovery ranges from 83.82% to 96.74%.Good reproducibility was obtained with RSD ranging from 1.68% to 4.18%.The results of the experiment showed that the analytical method is rapid,simple and accurate.It is suitable for analysis of chemical compounds of volatile oil in Ligusticum Chuanxiong Hort. |
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| Keywords: | aromatics volatile oil of Ligusticum Chuanxiong Hort quantitative analysis |
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