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C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究
引用本文:王 浩,周卿军,简 科,邵长伟,朱旖华.C/SiC复合材料有序多孔陶瓷接头的制备及其连接技术研究[J].无机材料学报,2013,28(7):763-768.
作者姓名:王 浩  周卿军  简 科  邵长伟  朱旖华
作者单位:(国防科学技术大学 新型陶瓷纤维及其复合材料重点实验室, 长沙 410073)
基金项目:国家自然科学基金(50702075, 51172280); 湖南省杰出青年基金(12JJ1008); 湖南省高校科技创新团队支持计划(2012)
摘    要:采用stöber法制备出单分散氧化硅小球, 并以此为模板, 结合先驱体转化技术成功制备出C/SiC复合材料纳米有序多孔陶瓷接头, 并对该接头制备工艺条件作了优化。对制备出的C/SiC多孔陶瓷接头分别采用先连后浸法(SJM)和直接浸渍法(DSM)进行了连接。结果显示, 两种方法连接的连接件的抗弯强度分别达82.4和20.5 MPa, 表明C/SiC多孔陶瓷接头采用SJM连接较好。

关 键 词:C/SiC复合材料  连接  先驱体转化技术  模板技术  有序多孔陶瓷接头  
收稿时间:2012-09-13
修稿时间:2012-12-01

Preparation of Ordered Porous Ceramic Joint on C/SiC Composites and Its Joining Technique
WANG Hao,ZHOU Qing-Jun,JIAN Ke,SHAO Chang-Wei,ZHU Yi-Hua.Preparation of Ordered Porous Ceramic Joint on C/SiC Composites and Its Joining Technique[J].Journal of Inorganic Materials,2013,28(7):763-768.
Authors:WANG Hao  ZHOU Qing-Jun  JIAN Ke  SHAO Chang-Wei  ZHU Yi-Hua
Affiliation:(Science and Technology on Advanced Ceramic Fibers and Composites Laboratory, National University of Defense Technology, Changsha 410073, China)
Abstract:Mono-dispersed silica spheres were prepared as template by st?ber method. Based on this template, the ordered nanoporous ceramic joints on the C/SiC composites were successfully fabricated for the first time by preceramic polymer techniques and the condition was optimized. Two different joining methods, directly soaking (DSM) and soaking after the first joining (SJM), were used for joining the ordered nanoporous ceramic joints of the C/SiC composites. The result shows that the bending strength of the joints by DSM and SJM is about 20.5 and 82.4 MPa, respectively, suggesting SJM more suitable for joining C/SiC composites.
Keywords:C/SiC composites  joining  precursor conversion technique  template technique  ordered nanoporous ceramic joint  
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