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Thermogravimetric method for determination of oxygen stoichiometry in superconducting 1:2:3 and metal-substituted 1:2:3 compounds
Authors:R Venkataramani  S P Garg  S Mazumder
Affiliation:(1) Physical Metallurgy Division, Bhabha Atomic Research Centre, 400 085 Bombay, India;(2) Neutron Physics Division, Bhabha Atomic Research Centre, 400 085 Bombay, India
Abstract:The paper presents a modified thermogravimetric method for determination of oxygen stoichiometry of the oxide superconductors YBa2Cu3O7−δ and metal-substituted compounds of the type YBa2−x La x Cu3O7+δ and YBa2(Cu1−x M x )3O7−δ (M=Mg/Zn) between 25° and 930°C.
Keywords:Thermogravimetry  stoichiometry
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