Synthesis and characterization of polycationic chitosan-graft-poly (l-lysine) |
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Authors: | Ping Chi |
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Affiliation: | State Key Laboratory of Bioreactor Engineering, and Engineering Research Center for Biomedical Materials of Ministry of Education, East China University of Science and Technology, Shanghai 200237, PR China |
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Abstract: | A type of polysaccharide/polypeptide hydride material, chitosan derivatives with polypeptide side chains, was prepared via ring-opening polymerization of Nε-carbobenzyloxy-l-lysine NCA initiated by water-soluble chitosan and followed by removing the side-chain protective groups. The graft polymer was investigated through FTIR spectroscopy, proton nuclear magnetic resonance spectroscopy and X-ray diffraction to confirm the structure. Furthermore, the results of the atomic force microscopy (AFM) measurement indicated the chitosan-graft-poly (l-lysine) was a kind of extraordinary polycation. |
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Keywords: | Atomic force microscopy Chitosan Polymer Poly (l-lysine) Polyelectrolyte |
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