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正交实验用于煤沥青基活性炭的工艺优化
引用本文:王晓瑞,钱仁渊,金鸣林. 正交实验用于煤沥青基活性炭的工艺优化[J]. 煤化工, 2005, 33(2): 16-19
作者姓名:王晓瑞  钱仁渊  金鸣林
作者单位:南京工业大学化学化工学院,210009;上海应用技术学院,200235
基金项目:上海市教委基金(02HK06)
摘    要:介绍了正交实验法用于煤沥青基活性炭的研制,在固定碱炭比的条件下,分析了炭化温度(A)、炭化时间(B)、活化温度(C)及活化时间(D)四因素对活性炭比表面积的影响。通过直观分析和方差分析可知,四因素中对BET比表面积影响次序为:B>D>A>C,从而找出制备煤沥青基活性炭的最优工艺条件A3B1C1D2,并且在炭化温度为450℃、炭化时间为30min、活化温度为800℃和活化时间为100min的条件下制备出比表面积为1846m2/g的活性炭。

关 键 词:正交实验  活性炭  煤沥青  比表面积
文章编号:1005-9598(2005)-02-0016-04
修稿时间:2004-12-10

Optimizing the Technology of Coal Tar Pitch-based Active Carbon with Orthogonal Experiment
Wang Xiaorui,Qian Renyuan,Jin Minglin. Optimizing the Technology of Coal Tar Pitch-based Active Carbon with Orthogonal Experiment[J]. Coal Chemical Industry, 2005, 33(2): 16-19
Authors:Wang Xiaorui  Qian Renyuan  Jin Minglin
Affiliation:Wang Xiaorui1,Qian Renyuan1 and Jin Minglin2
Abstract:The orthogonal experiment was applied in the research of coal tar pitch-based active carbon. The influence of carbonization temperature (A), carbonization time (B), activation temperature (C) and activation time (D) on specific surface area under fixed ratio of alkali/carbon was analyzed. It can be known by intuitionistic analysis and variance analysis that B>D>A>C. The optimum technology found out from the orthogonal test data was as follows: A3B1C1D2, and the active carbon with specific surface area of 1 846 m2/g was produced under the conditions of carbonization temperature of 450℃, carbonization time of 30min, activation temperature of 800℃ and activation time of 100min.
Keywords:orthogonal experiment  active carbon  coal tar pitch  specific surface area
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