| 硝酸铜氧化安息香制备苯偶酰 |
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| 引用本文： | 文瑞明,丁亮中,罗新湘,俞善信. 硝酸铜氧化安息香制备苯偶酰[J]. 化工学报, 2003, 54(1): 135-136 |
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| 作者姓名： | 文瑞明 丁亮中 罗新湘 俞善信 |
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| 作者单位： | DepartmentofChemistry,HunanCityUniversity,Yiang413049,Hunan,China |
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| 基金项目： | 湖南省自然科学基金，湖南省教育厅科研项目 |
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| 摘 要： | INTRODUCTIONBenzil is an important photosensitive initiator of organic synthesis intermediates, medicinal intermediates and ultraviolet solidified resin(UV resin), and is usually prepared by oxidizing benzoin. The oxidizers and methods reported are mainly: (PhCH2Et3N)+Br-/(PhCO)2O2/MeCN[1], DMSO/(COCl)2/CH2Cl2[2], CrO3*CH3NH2*HCl/Al2O3[3], the metallorganic compound[4], microwave radiation[5],etc.
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| 关 键 词： | 硝酸铜 氧化 安息香 苯偶酰 合成 |
| 收稿时间： | 2002-08-27 |
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PREPARATION OF BENZIL BY OXIDIZING BENZOIN WITH CUPRIC NITRATE |
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| WEN Ruiming,DING Liangzhong,LUO Xinxiang,YU Shanxin. PREPARATION OF BENZIL BY OXIDIZING BENZOIN WITH CUPRIC NITRATE[J]. Journal of Chemical Industry and Engineering(China), 2003, 54(1): 135-136 |
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| Authors: | WEN Ruiming DING Liangzhong LUO Xinxiang YU Shanxin |
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| Affiliation: | Department of Chemistry,Hunan City University, Yiyang 413049, Hunan, China;Department of Chemistry,Hunan City University, Yiyang 413049, Hunan, China;Department of Chemistry,Hunan City University, Yiyang 413049, Hunan, China;Department of Chemistry,Hunan City University, Yiyang 413049, Hunan, China |
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| Abstract: | INTRODUCTION Benzil is an important photosensitive initiator of organic synthesis intermediates, medicinal intermediates and ultraviolet solidified resin(UV resin), and is usually prepared by oxidizing benzoin. The oxidizers and methods reported are mainly: (PhCH2Et3N)+Br-/(PhCO)2O2/MeCN[1], DMSO/(COCl)2/CH2Cl2[2], CrO3*CH3NH2*HCl/Al2O3[3], the metallorganic compound[4], microwave radiation[5],etc. |
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| Keywords: | benzil benzoin cupric compound cupric nitrate oxidation |
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