| 对乙烯基苯甲酸的合成 |
| |
| 引用本文： | 方卫国. 对乙烯基苯甲酸的合成[J]. 浙江化工, 2010, 41(4): 7-9 |
| |
| 作者姓名： | 方卫国 |
| |
| 作者单位： | 杭州澳赛诺化工有限公司,浙江,杭州,311604 |
| |
| 摘 要： | 以对溴苯甲酸为原料,经格氏试剂交换反应得到格氏试剂,然后与乙醛加成合成对羟乙基苯甲酸,再经脱水反应合成了标题化合物。产品总收率47.0%,产品纯度99.4%。通过1HMNR对产品进行了表征。
|
| 关 键 词： | 对乙烯基苯甲酸 对溴苯甲酸 脱水 合成 |
Study on Synthesis of 4-Vinylbenzoic Acid |
| |
| FANG Wei-guo. Study on Synthesis of 4-Vinylbenzoic Acid[J]. Zhejiang Chemical Industry, 2010, 41(4): 7-9 |
| |
| Authors: | FANG Wei-guo |
| |
| Affiliation: | FANG Wei-guo (Hangzhou Allsino Chemicals Co.,Ltd. Hangzhou 311604,China) |
| |
| Abstract: | 4-Vinylbenzoic acid was synthesized by using 4-bromobenzoic acid and acetaldehyde as the starting materials with its purity reaching 99.4% at an overall yield of 47.0% ,structure of the product was confirmed by 1HNMR. |
| |
| Keywords: | 4-vinylbenzoic acid 4-bromobenzoic acid dehydration synthesis |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
