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SYNTHESIS AND CHARACTERIZATION OF A NEW NIOBATE: Sr6Ti7Nb9O42
Authors:ZHANG Hui  FANG Liang  XIE Jiren  WU Bolin  YUAN Runzhang
Affiliation:ZHANG Hui FANG Liang XIE Jiren WU Bolin YUAN Runzhang Wuhan University of Technology
Abstract:A new niabate Sr6Ti7Nb9O42 was synthesized for the first time by solid state reaction in SrO-TiO2-Nb2O5 ternary system. The new compound was characterized by EPMA, XRD, SEM and DTA. The X-ray powder diffraction data of Sr6Ti7Nb9O42 were firstly reported in the paper. Sr6Ti7Nb9O42 crystallizes the hexagonal system with unit cell parameters a=8.9991(4) A,c= 11.5118(9)A. and space group P6/mcm (193), z=1. The calculated and measured densities are 4. 783 g/cm3 and 4. 764 g/cm3, respectively.
Keywords:SrO-TiO2-Nb2O5 system  niobate  X-ray powder diffraction
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