| 苦参总碱分离纯化方法的研究 |
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| 引用本文： | 胡艳丽,郭丽,贾晓红.苦参总碱分离纯化方法的研究[J].食品科学,2007,28(1):32-36. |
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| 作者姓名： | 胡艳丽 郭丽 贾晓红 |
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| 作者单位： | 新疆特种植物药资源教育部重点实验室； 安徽农业大学茶与食品科技学院； 新疆农业大学食品科学学院 新疆石河子832002； 安徽合肥230036； 新疆乌鲁木齐830052； |
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| 摘 要： | 本文旨在研究一种分离苦参总碱的最佳纯化方法。经实验,确定氧化铝柱分离法与重结晶法相结合的方法是分离和纯化总碱中各组分的最佳有效方法,并通过高效液相色谱对本实验所得到的苦参碱和氧化苦参碱结晶物进行纯度分析,确定这两种生物碱结晶物纯度均高于98%。
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| 关 键 词： | 苦参总碱 氧化苦参碱 苦参碱 分离纯化 |
| 文章编号： | 1002-6630（2007）01-0032-05 |
| 修稿时间： | 2005-11-16 |
Study on Separation and Purification Technology of Sophora alopecuroides L. |
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| HU Yan-li,GUO Li,JIA Xiao-hong.Study on Separation and Purification Technology of Sophora alopecuroides L.[J].Food Science,2007,28(1):32-36. |
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| Authors: | HU Yan-li GUO Li JIA Xiao-hong |
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| Affiliation: | 1.Key Laboratory of Xinjiang Phytomedicine Resources, Ministry of Education, Shihezi 832002, China; 2.School of Tea and Food Science and Technology, Anhui Agricultural University, Hefei 230036, China; 3.School of Food Science, Xinjiang Agricultural University, Urumqi 830052, China |
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| Abstract: | The aim of this paper was to research an optimumly separated and purified method of Sophora alopecuroides L. The results of experiment determined that the most effective separating and purifing method for each ingredient in Sophora alopecuroides L. was a combined one by using alumina column followed recrystallization. Besides, the matrine and oxymatrine crystals obtained respectively from this experiment were analysed for their purification by high performance liquid chromatog- raphy (HPLC). Finally, we found that the purities of the two pured alkaloids both exceed 98%. |
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| Keywords: | Sophora alopecuroides L oxymatrine matrine separation and purification |
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