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GC-PFPD法分析1-丁烯碳四原料中的微量硫化合物
引用本文:范晏春.GC-PFPD法分析1-丁烯碳四原料中的微量硫化合物[J].广州化工,2012,40(20):89-90,102.
作者姓名:范晏春
作者单位:中国石油化工股份有限公司广州分公司,广东广州,510726
摘    要:利用毛细管色谱柱、脉冲火焰光度检测器及各种形态硫的渗透管,建立了对中石化广州分公司MTBE联产丁烯-1所需的炼厂碳四中的微量有机硫化物的分析方法。此方法可以准确定量含量低至84μg/kg的H2S、44μg/kg的COS和68μg/kg的MeSH。该方法具有操作简便、灵敏度高等优点,适于炼厂碳四原料中微量硫化物的分析测定。

关 键 词:微量形态硫  气相色谱法  脉冲火焰光度检测器  炼厂碳四原料  外标法

Analysis of Trace Sulfur Compounds in the Four-carbon Raw Materials for 1-Butene by GC-PFPD
FAN Yan-chun.Analysis of Trace Sulfur Compounds in the Four-carbon Raw Materials for 1-Butene by GC-PFPD[J].GuangZhou Chemical Industry and Technology,2012,40(20):89-90,102.
Authors:FAN Yan-chun
Affiliation:FAN Yan-chun(Guangzhou Petrochemical Branch Company,SINOPEC,Guangdong Guangzhou 510726,China)
Abstract:The use of capillary column,pulsed flame photometric detector and the sulfide permeation tube,established a Guangzhou branch of Sinopec MTBE required cogeneration refinery 1-butene plant carbon in four of the analysis of trace organic sulfide method.This method was an accurate quantitative analysis can be as low as 84 μg/kg content of H2S,44μg/kg content of COS,and 68 μg/kg content of MeSH.The method was simple,high sensitivity,suitable for determining the morphology of trace sulfur compounds and detecting the composition trace sulfur compounds.
Keywords:sulfide permeation tube  pulsed flame photometric detector  trace sulfur compounds  materials carbon four  external standard method
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