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Particle size measurement of reference particle candidates and uncertainty region of count and mass based cumulative distribution
Affiliation:1. Department of Chemical Engineering, Hiroshima University, 1-4-1, Kagamiyama, Higashi-Hiroshima, Hiroshima 739-8527, Japan;2. Department of Chemical Engineering and Materials Science, Doshisha University, 1-3 Tatara Miyakodani, Kyotanabe, Kyoto 630-0321, Japan;3. Kyoto University, Invited Special Research Fellow, Cooperative Research Center of Life Sciences, Kobe Gakuin University, Minatojima, Chuou-ku, Kobe 650-8586, Japan;4. Horiba, Co., Ltd., 2 Miyanohonmachi, Kisshoin, Minami-ku, Kyoto 601-8510, Japan
Abstract:In order to confirm reliable particle size measurement technique and to prepare standard reference particles for calibrating particle size measurement devices, uncertainty region of count and mass based size distribution have been theoretically examined. The uncertainty region of count base cumulative size distribution is smaller than that of the mass base cumulative distribution.The uncertainty region of count base cumulative size distribution is nearly constant over wide range of particle diameter and the region is nearly constant for sample size greater than about 20,000.On the other hand, the uncertainty region of mass base cumulative distribution increases with the increase of particle diameter.The reliability of theoretical uncertainty region is confirmed by the experimental data of particle size measurement.
Keywords:Particle size  Reference particle  Uncertainty region  Log-normal distribution  Size measurement
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