| 气相色谱与硫化学发光检测器联用测定芳烃样品中的环丁砜 |
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| 引用本文： | 聂兆丰. 气相色谱与硫化学发光检测器联用测定芳烃样品中的环丁砜[J]. 广东化工, 2005, 32(8): 76-78 |
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| 作者姓名： | 聂兆丰 |
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| 作者单位： | 中国石油化工股份有限公司,广州分公司检验中心,广东,广州,510726 |
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| 摘 要： | 采用气相色谱和硫化学发光检测器（GC-SCD）技术，通过直接进样测定芳烃样品中环丁砜。本方法用六个不同浓度的定量标准样品，得到的定量标准曲线的相关性≥0．9999；在回收试验中，得到的回收率在95％～109％范围内；对抽余油进行5次重复性试验，环丁砜含量测定结果RSD仅为2．5％。
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| 关 键 词： | 环丁砜 硫化学发光检测器 气相色谱 定量 |
| 修稿时间： | 2005-08-13 |
Determination of Sulfones by Gas Chromatography with Sulfur Chemiluminescence Deterctor |
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| Nie Zhaofeng. Determination of Sulfones by Gas Chromatography with Sulfur Chemiluminescence Deterctor[J]. Guangdong Chemical Industry, 2005, 32(8): 76-78 |
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| Authors: | Nie Zhaofeng |
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| Abstract: | This paper introduced the application of gas chromatography with sulfur chemiluminescence detector.With this method we can catch the content of sulfones in samples from aromatic extraction unit by a single injection.The chromatography and the detection system exhibited good precision,linearity,selectivity and sensitivity.In the detection of sulfones,we can receive that correlation coefficient was over 0.9999,recovery was in the rang of 95%~109% and the relative standard deviation was only 2.5%. |
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| Keywords: | sulfone sulfur chemiluminescence detector gas chromatography quantify |
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