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用于低浓度NO2精确测量的傅里叶变换红外光谱系统研究
引用本文:李剑,王德发,夏春,马浩淼,王漫,王振,黄鹏.用于低浓度NO2精确测量的傅里叶变换红外光谱系统研究[J].计量学报,2019,40(3):517-521.
作者姓名:李剑  王德发  夏春  马浩淼  王漫  王振  黄鹏
作者单位:青岛市计量技术研究院,山东青岛,266101;中国计量科学研究院,北京,100029
基金项目:国家重点研发计划(2016YFF0201101); 国家标准物质资源共享平台(28-APT1702-14)
摘    要:建立了一套可精确测量低浓度NO2的傅里叶变换红外光谱系统(Fourier transform infrared spectrometer, FTIR)。运用该系统测量动态稀释法得到的不同浓度的标准气体中的NO2的浓度,显示出该系统具有良好的线性响应, 并以此建立了该系统的校准方程。比对试验证明了该系统的测量结果准确可靠; 稳定性研究则显示该系统具有良好的长期稳定性。

关 键 词:计量学  NO2监测  FTIR  动态稀释法  标准气体
收稿时间:2017-10-12

Research on a FTIR System for Accurate Measurement of Low Concentration NO2
LI Jian,WANG De-fa,XIA Chun,MA Hao-miao,WANG Man,WANG Zhen,HUANG Peng.Research on a FTIR System for Accurate Measurement of Low Concentration NO2[J].Acta Metrologica Sinica,2019,40(3):517-521.
Authors:LI Jian  WANG De-fa  XIA Chun  MA Hao-miao  WANG Man  WANG Zhen  HUANG Peng
Affiliation:1.Qingdao Institute of Measurement Technology, Qingdao, Shandong 266101, China
2.National Institute of Metrology, Beijing 100029, China
Abstract:A FTIR system for the accurate measurement of low concentration NO2 was developed. By using the proposed syestem, the concentration of NO2 in the different standard gas were measured; the standard gas were obtained by dynamic dilution method. It was indicated that the system has a good linear response, thus the calibration equation of the system was established. The comparison test showed that the system is accurate and reliable. The stability study showed that the system has good long-term stability. By using dynamic dilution method based on mass flow controllers, the standard gases with different concentration were obtained. This system has a calibration curve with good linearity. The comparison test shows that the system is accurate and reliable. The stability study shows that the system has good long-term stability.
Keywords:metrology  NO2 monitoring  FTIR  dynamic dilution method  standard gas  
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