| 微波辐射下NKC-9树脂催化合成1-萘乙酸甲酯 |
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| 引用本文： | 胡思前,陈明,陈荷连.微波辐射下NKC-9树脂催化合成1-萘乙酸甲酯[J].化工中间体,2006(10):15-18. |
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| 作者姓名： | 胡思前 陈明 陈荷连 |
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| 作者单位： | 江汉大学,化学与环境工程学院,湖北,武汉,430056 |
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| 摘 要： | 以NKC-9阳离子交换树脂为催化剂,在微波条件下用1-萘乙酸和甲醇合成1-萘乙酸甲酯.最佳合成条件为:醇酸摩尔比为14:1,催化剂为1-萘乙酸的80%,微波辐射时间为15分钟,微波功率为600瓦,产率为80.48%.
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| 关 键 词： | 1-萘乙酸 合成 微波辐射 阳离子交换树脂 1-萘乙酸甲酯 |
| 文章编号： | 1006-253x(2006)10-015-4 |
| 收稿时间： | 07 20 2006 12:00AM |
| 修稿时间： | 2006年7月20日 |
Synthesis of Methyl 1-Naphthylacetate with NKC-9 Resin as Catalyst under Microwave Irradiation |
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| Authors: | HU Si-qian CHEN Ming CHEN He-lian |
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| Affiliation: | School of Chemistry and Environmental Engineering, Jianghan University, Wuhan 430056,Hubei |
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| Abstract: | The methyl 1-naphthylacetate was synthesized by 1-naphthylene acetic acid and methanol with NKC-9 resin as catalyst under microwave irradiation. The optimum reaction conditions were as follows: the mole ratio of alcohol to carboxylic acid was 14:1, the catalyst was 80% of 1-naphthyl acetic acid, the reaction time was 15min, the microwave power was 600 w, the yield was 80.48%. |
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| Keywords: | 1-naphthylacetic acetic acid synthesis microwave irradiation NKC-9 resin methyl 1-naphthylacetate |
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