| 离子液体Et3NHCl-xAlCl3催化合成苯基二氯化膦研究 |
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| 引用本文： | 刘方,唐旭东,张家鹤.离子液体Et3NHCl-xAlCl3催化合成苯基二氯化膦研究[J].广西化工,2009(2):4-5. |
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| 作者姓名： | 刘方 唐旭东 张家鹤 |
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| 作者单位： | 天津科技大学材料科学与化学工程学院,天津300457 |
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| 摘 要： | 按文献方法合成了不同x值的Et3NHCl-xAlCl3离子液体，并将其用于催化合成苯基二氯化膦，研究了离子液体酸性、用量对反应活性的影响，对其重复使用性进行了考察，并对合成的苯基二氯化膦进行了红外表征。
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| 关 键 词： | 离子液体 催化 苯基二氯化膦 |
Synthesis of Dichlorophenylphosphine Catalyzed by Et3NHCl-xAlCl3 Ionic Liquids |
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| LIU Fang,TANG Xu-Dong,ZHANG Jia-He.Synthesis of Dichlorophenylphosphine Catalyzed by Et3NHCl-xAlCl3 Ionic Liquids[J].Guangxi Chemical Industry,2009(2):4-5. |
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| Authors: | LIU Fang TANG Xu-Dong ZHANG Jia-He |
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| Affiliation: | (School of Material Science ＆ Chemical Engineering, Tianjin University of Science ＆ Techology, Tianjin 300457, China) |
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| Abstract: | Et3NHCl-xAlCl3 ionic liquids with different value of x were prepared according to the reference, and the products were used for the catalytic synthesis of dichlorophenylphosphine（DCPP）. The effect of acidity and dosages of ionic liquids on the reaction activity was studied, its capacity of reusing was investigated, and the FT- IR was used to analyze the synthesized DCPP. |
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| Keywords: | ionic liquids catalysis dichlorophenylphosphine（DCPP） |
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