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CuO nano-whiskers: Electrodeposition,Raman analysis,photoluminescence study and photocatalytic activity
Authors:Nillohit Mukherjee  Bibhutibhushan Show  Swarup Kumar Maji  Utpal Madhu  Sanjib Kumar Bhar  Bibhas Chandra Mitra  Gobinda Gopal Khan  Anup Mondal
Affiliation:1. Department of Chemistry, Bengal Engineering and Science University, Botanic Garden, Howrah 711103, India;2. Department of Chemistry, Jadavpur University, Kolkata 700032, India;3. Department of Chemistry, Vivekananda College, Thakurpukur, Kolkata 700063, India;4. Department of Physics, Bengal Engineering and Science University, Botanic Garden, Howrah 711103, India;5. Department of Material Sciences, S. N. Bose National Centre for Basic Sciences, Sector-III, Block JD, Salt Lake, Kolkata 700098, India;1. Laboratory of Nanoscience and Technology, Department of Physics, International Islamic University, H-10, Islamabad, Pakistan;2. Departments of Bioinformatics and Biotechnology, International Islamic University, Islamabad, Pakistan;3. Institute of Biomedical and Genetic Engineering (IBGE), Islamabad, Pakistan;4. Experimental Physics Labs, National Center for Physics, Islamabad 44000, Pakistan;5. UNESCO-UNISA Africa Chair in Nanosciences/Nanotechnology, College of Graduate Studies, University of South Africa, Muckleneuk ridge, POBox 392, Pretoria, South Africa;6. Nanosciences African Network (NANOAFNET), iThemba LABS-National Research Foundation, 1 Old Faure road, Somerset West 7129, POBox 722, Somerset West, Western Cape Province, South Africa;1. Chemistry Department, Faculty of Sciences, Shahid Rajaee Teacher Training University, PO Box 16785-163, Tehran, Iran;2. Department of Chemistry, Yadegar-e-Imam Khomeini (RAH) Branch, Islamic Azad University, Tehran, Iran;1. Department of Chemistry, Faculty of Science, University of Guilan, P.O. Box 1914, Rasht, Iran;2. Department of Chemistry, Faculty of Science, Payam_Noor University, Ardabil, Iran;1. School of Physics and Electronic Electrical Engineering, Huaiyin Normal University, Huai’an 223300, PR China;2. Huaian Key Laboratory of Functional Materials for Informatics, Huai’an 223300, PR China
Abstract:An electrochemical route to synthesize CuO thin films with nano-whiskers like structure, from a metallic Cu precursor is reported. Structural characterization showed the formation of cubic phase for both the Cu and CuO films, whereas, the grains were found to change their shapes from cubic to nano-whiskers as an effect of annealing (in air at 600 °C for 30 min). X-ray diffraction (XRD), scanning electron microscopy (SEM), UV–vis, Photoluminescence (PL) and Raman analyses were carried out with the films. The photocatalytic activity of the prepared CuO films was determined by measuring the degradation of Rose Bengal (RB) dye, to find out its potential application in waste water treatment.
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